C₅₄H₇₈N₆O₉

Base Information

Chemical Name:C₅₄H₇₈N₆O₉
CAS No.:1388842-07-6
Molecular Formula:C₅₄H₇₈N₆O₉
Molecular Weight:955.248
Hs Code.:

C<sub>54</sub>H<sub>78</sub>N<sub>6</sub>O<sub>9</sub>

Synonyms:

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Chemical Property of C₅₄H₇₈N₆O₉

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Technology Process of C₅₄H₇₈N₆O₉

There total 9 articles about C₅₄H₇₈N₆O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124818-94-6,116246-06-1
ethyl (2E,4S)-4-[(tert-butoxycarbonyl)amino]-5-phenylpent-2-enoate

: 1388842-07-6
C₅₄H₇₈N₆O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluoroacetic acid / dichloromethane / 0.5 h / Cooling with ice

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C

2.2: 6 h / 0 - 20 °C

3.1: trifluoroacetic acid / dichloromethane / 0.5 h / Cooling with ice

4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C

4.2: 8 h / 0 - 20 °C

5.1: palladium on carbon; hydrogen / ethanol / 6 h

With palladium on carbon; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc32911e

Reference yield:

: 72155-45-4
Boc-L-phenylalaninal

: 1388842-07-6
C₅₄H₇₈N₆O₉

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrahydrofuran / 5 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane / 0.5 h / Cooling with ice

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C

3.2: 6 h / 0 - 20 °C

4.1: trifluoroacetic acid / dichloromethane / 0.5 h / Cooling with ice

5.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C

5.2: 8 h / 0 - 20 °C

6.1: palladium on carbon; hydrogen / ethanol / 6 h

With palladium on carbon; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; 1.1: Wittig reaction;
DOI:10.1039/c2cc32911e

Reference yield:

: 244033-75-8
(S)-(+)-trans-5-phenyl-4-amino-2-pentenoic acid ethyl ester

: 1388842-07-6
C₅₄H₇₈N₆O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C

1.2: 6 h / 0 - 20 °C

2.1: trifluoroacetic acid / dichloromethane / 0.5 h / Cooling with ice

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C

3.2: 8 h / 0 - 20 °C

4.1: palladium on carbon; hydrogen / ethanol / 6 h

With palladium on carbon; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc32911e