bis(dicyclohexylphenylphosphane)-sulfur dioxide-nickel⁽⁰⁾

Base Information

• Chemical Name: bis(dicyclohexylphenylphosphane)-sulfur dioxide-nickel⁽⁰⁾
• CAS No.: 137865-16-8
• Molecular Formula: C₃₆H₅₄NiO₂P₂S
• Molecular Weight: 671.527
• Mol file: 137865-16-8.mol

Synonyms:

Chemical Property of bis(dicyclohexylphenylphosphane)-sulfur dioxide-nickel⁽⁰⁾

Chemical Property:

Purity/Quality:

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Technology Process of bis(dicyclohexylphenylphosphane)-sulfur dioxide-nickel⁽⁰⁾

There total 1 articles about bis(dicyclohexylphenylphosphane)-sulfur dioxide-nickel⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

bis(1,5-cyclooctadiene)nickel (0) (1295-35-8) + sulfur dioxide (7446-09-5,12143-17-8,89125-89-3) + dicyclohexylphenylphosphine (6476-37-5) → bis(dicyclohexylphenylphosphane)-sulfur dioxide-nickel(0) (137865-16-8,119509-17-0)

Guidance literature:

In tetrahydrofuran; SO2 was passed through a dark red soln. of Ni(COD)2 and PPhCy2 (molar ratio > 1:3) in THF (color of the soln. changed to red-orange), concn. of soln., pptn. after 4 days; elemental analysis;

upstream raw materials:

bis(1,5-cyclooctadiene)nickel ⁽⁰⁾

sulfur dioxide

dicyclohexylphenylphosphine