C₆₂H₅₇⁽²⁾H₇O₁₃Si

Base Information

Chemical Name:C₆₂H₅₇⁽²⁾H₇O₁₃Si
CAS No.:1315508-09-8
Molecular Formula:C₆₂H₆₄O₁₃Si
Molecular Weight:1052.21
Hs Code.:

C<sub>62</sub>H<sub>57</sub><sup>(2)</sup>H<sub>7</sub>O<sub>13</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₂H₅₇⁽²⁾H₇O₁₃Si

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Technology Process of C₆₂H₅₇⁽²⁾H₇O₁₃Si

There total 10 articles about C₆₂H₅₇⁽²⁾H₇O₁₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1012037-70-5
ethyl 3,4-dihydro-5,6,8-trimethoxy-3,4-dioxonaphthalene-2-carboxylate

: 1315508-09-8
C₆₂H₅₇⁽²⁾H₇O₁₃Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium dithionite; water / benzene / 0.08 h

2.1: potassium carbonate / 6 h / Reflux

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C

4.1: Dess-Martin periodane / dichloromethane / 1 h

5.1: ammonium acetate / 0.5 h / Reflux

6.1: sodium tetrahydroborate / methanol; chloroform / 0.08 h

6.2: pH 3

7.1: phenyl isocyanate; triethylamine / benzene / 17 h / 65 - 70 °C

8.1: hydrogen; boric acid / tetrahydrofuran; methanol; water / 8 h

9.1: 1H-imidazole / N,N-dimethyl-formamide / 18 h / Inert atmosphere

10.1: triethylamine

With 1H-imidazole; sodium tetrahydroborate; lithium aluminium tetrahydride; sodium dithionite; ammonium acetate; water; hydrogen; boric acid; potassium carbonate; Dess-Martin periodane; phenyl isocyanate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo200399z

Reference yield:

: C₁₆H₁₈O₇

: 1315508-09-8
C₆₂H₅₇⁽²⁾H₇O₁₃Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / 6 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C

3.1: Dess-Martin periodane / dichloromethane / 1 h

4.1: ammonium acetate / 0.5 h / Reflux

5.1: sodium tetrahydroborate / methanol; chloroform / 0.08 h

5.2: pH 3

6.1: phenyl isocyanate; triethylamine / benzene / 17 h / 65 - 70 °C

7.1: hydrogen; boric acid / tetrahydrofuran; methanol; water / 8 h

8.1: 1H-imidazole / N,N-dimethyl-formamide / 18 h / Inert atmosphere

9.1: triethylamine

With 1H-imidazole; sodium tetrahydroborate; lithium aluminium tetrahydride; ammonium acetate; hydrogen; boric acid; potassium carbonate; Dess-Martin periodane; phenyl isocyanate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo200399z

Reference yield:

: 1315508-06-5
7,8-dibenzyloxy-6-[3-(3,4-dibenzyloxy-5,6,8-trimethoxynaphthalen-2-ylmethyl)-4,5-dihydroisoxazol-5-yl]-1-oxo-1H-isochromene-3-carboxylic acid methyl ester

: 1315508-09-8
C₆₂H₅₇⁽²⁾H₇O₁₃Si

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; boric acid / tetrahydrofuran; methanol; water / 8 h

2: 1H-imidazole / N,N-dimethyl-formamide / 18 h / Inert atmosphere

3: triethylamine

With 1H-imidazole; hydrogen; boric acid; triethylamine; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo200399z