methoxy(phenyl){tris(trimethylsilyl)methyl}borane

Base Information

Chemical Name:methoxy(phenyl){tris(trimethylsilyl)methyl}borane
CAS No.:124044-73-1
Molecular Formula:C₁₇H₃₅BOSi₃
Molecular Weight:350.532
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methoxy(phenyl){tris(trimethylsilyl)methyl}borane

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Technology Process of methoxy(phenyl){tris(trimethylsilyl)methyl}borane

There total 1 articles about methoxy(phenyl){tris(trimethylsilyl)methyl}borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 87122-54-1
dimethoxy{tris(trimethylsilyl)methyl}borane

: 591-51-5
phenyllithium

: 124044-73-1
methoxy(phenyl){tris(trimethylsilyl)methyl}borane

Guidance literature:: In diethyl ether; benzene; soln. of C6H5Li (benzene/diethyl ether 1:1) added to a soln. of (MeO)2BC(SiMe3)3 in diethyl ether at -78°C, refluxed for 4 h, (O2 free and dry medium); evapn. to dryness, extd. (hexane), solvent removed, sublimed (110°C/0.005 Torr); elem. anal.;