methyl 2,5-di-O-benzoyl-3-deoxy-α-D-threo-pentofuranoside

Base Information

Chemical Name:methyl 2,5-di-O-benzoyl-3-deoxy-α-D-threo-pentofuranoside
CAS No.:26532-13-8
Molecular Formula:C₂₀H₂₀O₆
Molecular Weight:356.375
Hs Code.:

Synonyms:

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Chemical Property of methyl 2,5-di-O-benzoyl-3-deoxy-α-D-threo-pentofuranoside

Chemical Property:

Purity/Quality:

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Technology Process of methyl 2,5-di-O-benzoyl-3-deoxy-α-D-threo-pentofuranoside

There total 13 articles about methyl 2,5-di-O-benzoyl-3-deoxy-α-D-threo-pentofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79580-61-3,394739-29-8
tri-O-acetyl-D-lyxono-1,4-lactone

: 26532-13-8
methyl 2,5-di-O-benzoyl-3-deoxy-α-D-threo-pentofuranoside

Guidance literature:: Multi-step reaction with 5 steps

1: H₂, triethylamine / Pd/C / ethyl acetate / 28 h / 2280 Torr / Ambient temperature

2: 97 percent / aq. potassium hydroxide / ethanol

3: 75 percent / diisoamylborane / tetrahydrofuran / Ambient temperature

4: acetyl chloride / 20 h

5: 536 mg / pyridine

With pyridine; potassium hydroxide; diisoamyl borane; hydrogen; triethylamine; acetyl chloride; palladium on activated charcoal; In tetrahydrofuran; ethanol; ethyl acetate;

Reference yield:

: 15384-34-6
D-lyxono-1,4-lactone

: 26532-13-8
methyl 2,5-di-O-benzoyl-3-deoxy-α-D-threo-pentofuranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / aq. perchloric acid / 0.5 h / Ambient temperature

2: H₂, triethylamine / Pd/C / ethyl acetate / 28 h / 2280 Torr / Ambient temperature

3: 97 percent / aq. potassium hydroxide / ethanol

4: 75 percent / diisoamylborane / tetrahydrofuran / Ambient temperature

5: acetyl chloride / 20 h

6: 536 mg / pyridine

With pyridine; potassium hydroxide; perchloric acid; diisoamyl borane; hydrogen; triethylamine; acetyl chloride; palladium on activated charcoal; In tetrahydrofuran; ethanol; ethyl acetate;

Reference yield:

: 15384-37-9
D-xylono-1,4-lactone

: 26532-13-8
methyl 2,5-di-O-benzoyl-3-deoxy-α-D-threo-pentofuranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 42 percent / aq. perchloric acid / 0.5 h / Ambient temperature

2: H₂, triethylamine / Pd/C / ethyl acetate / 28 h / 2280 Torr / Ambient temperature

3: 97 percent / aq. potassium hydroxide / ethanol

4: 75 percent / diisoamylborane / tetrahydrofuran / Ambient temperature

5: acetyl chloride / 20 h

6: 536 mg / pyridine

With pyridine; potassium hydroxide; perchloric acid; diisoamyl borane; hydrogen; triethylamine; acetyl chloride; palladium on activated charcoal; In tetrahydrofuran; ethanol; ethyl acetate;