Technology Process of 5,5-Bis(3,3-dimethylbutyl)-2,2,8,8-tetramethylnonane
There total 4 articles about 5,5-Bis(3,3-dimethylbutyl)-2,2,8,8-tetramethylnonane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) sodium borohydride, boron fluoride etherate, 2.) H2O2, NaOH
2: 100 percent / HCl gas / CH2Cl2 / 2 h / Ambient temperature
3: 1.) triisobutylaluminium, 2.) methylchloride
With
hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; methylene chloride; boron trifluoride diethyl etherate; dihydrogen peroxide; triisobutylaluminum;
In
dichloromethane;
DOI:10.1021/jo00298a068
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) Mg / 1.) ether, 2.) reflux
2: 100 percent / HCl gas / CH2Cl2 / 2 h / Ambient temperature
3: 1.) triisobutylaluminium, 2.) methylchloride
With
hydrogenchloride; methylene chloride; triisobutylaluminum; magnesium;
In
dichloromethane;
DOI:10.1021/jo00298a068
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 100 percent / HCl gas / CH2Cl2 / 2 h / Ambient temperature
2: 1.) triisobutylaluminium, 2.) methylchloride
With
hydrogenchloride; methylene chloride; triisobutylaluminum;
In
dichloromethane;
DOI:10.1021/jo00298a068
