C₃₆H₄₃N₃O₅

Base Information

Chemical Name:C₃₆H₄₃N₃O₅
CAS No.:1447825-60-6
Molecular Formula:C₃₆H₄₃N₃O₅
Molecular Weight:597.755
Hs Code.:

C<sub>36</sub>H<sub>43</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₃₆H₄₃N₃O₅

Chemical Property:

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Technology Process of C₃₆H₄₃N₃O₅

There total 16 articles about C₃₆H₄₃N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1447825-91-3
C₂₇H₃₉NO₂SSi

: 1447825-60-6
C₃₆H₄₃N₃O₅

Guidance literature:: Multi-step reaction with 13 steps

1: tetrahydrofuran; dichloromethane / 0.67 h / 20 °C

2: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C

3: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C

4: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

5: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 14 h / 20 °C

6: triethylamine; diphenyl phosphoryl azide / dichloromethane / 17.33 h / 0 - 20 °C

7: 29 h / Reflux

8: potassium carbonate / methanol / 14 h / 20 °C

9: triethylamine / dichloromethane / 3 h / 0 - 20 °C

10: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

11: triethylamine / dichloromethane / 19 h / 0 - 20 °C

12: trifluoroacetic acid; palladium on activated charcoal; hydrogen / tetrahydrofuran / 1 h / 0 °C

13: triethylamine / dichloromethane / 1 h / 0 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; sodium carbonate; potassium carbonate; Dess-Martin periodane; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol; 1: |Grignard Reaction / 4: |Dess-Martin Oxidation / 7: |Curtius Rearrangement;
DOI:10.1021/jm400542h

Reference yield:

: 1447825-68-4
C₃₃H₃₉NO₄Si

: 1447825-60-6
C₃₆H₄₃N₃O₅

Guidance literature:: Multi-step reaction with 15 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.33 h / -78 °C

1.2: 1 h / 20 °C

2.1: copper(II) sulfate / dichloromethane / 22 h / 20 °C

3.1: tetrahydrofuran; dichloromethane / 0.67 h / 20 °C

4.1: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C

5.1: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C

6.1: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

7.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 14 h / 20 °C

8.1: triethylamine; diphenyl phosphoryl azide / dichloromethane / 17.33 h / 0 - 20 °C

9.1: 29 h / Reflux

10.1: potassium carbonate / methanol / 14 h / 20 °C

11.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

12.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

13.1: triethylamine / dichloromethane / 19 h / 0 - 20 °C

14.1: trifluoroacetic acid; palladium on activated charcoal; hydrogen / tetrahydrofuran / 1 h / 0 °C

15.1: triethylamine / dichloromethane / 1 h / 0 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; Dess-Martin periodane; copper(II) sulfate; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; toluene; tert-butyl alcohol; 3.1: |Grignard Reaction / 6.1: |Dess-Martin Oxidation / 9.1: |Curtius Rearrangement;
DOI:10.1021/jm400542h

Reference yield:

: 1447825-71-9
C₃₅H₄₉NO₂SSi

: 1447825-60-6
C₃₆H₄₃N₃O₅

Guidance literature:: Multi-step reaction with 12 steps

1: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C

2: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C

3: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

4: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 14 h / 20 °C

5: triethylamine; diphenyl phosphoryl azide / dichloromethane / 17.33 h / 0 - 20 °C

6: 29 h / Reflux

7: potassium carbonate / methanol / 14 h / 20 °C

8: triethylamine / dichloromethane / 3 h / 0 - 20 °C

9: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

10: triethylamine / dichloromethane / 19 h / 0 - 20 °C

11: trifluoroacetic acid; palladium on activated charcoal; hydrogen / tetrahydrofuran / 1 h / 0 °C

12: triethylamine / dichloromethane / 1 h / 0 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; sodium carbonate; potassium carbonate; Dess-Martin periodane; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol; 3: |Dess-Martin Oxidation / 6: |Curtius Rearrangement;
DOI:10.1021/jm400542h