Technology Process of C28H38F4N2O4S
There total 8 articles about C28H38F4N2O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dihydrogen peroxide / tetrahydrofuran; acetic acid / 6 h / 25 °C
2: trifluoroacetic acid / dichloromethane / 1 h / 25 °C
3: i-Amyl alcohol / 24 h / Reflux
4: sodium cyanoborohydride / methanol / 1 h / 25 °C
5: hydrogen; palladium 10% on activated carbon / methanol / 45 °C
With
palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; sodium cyanoborohydride; trifluoroacetic acid;
In
tetrahydrofuran; methanol; i-Amyl alcohol; dichloromethane; acetic acid;
DOI:10.1016/j.bmcl.2013.07.071
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium hydroxide / tetrahydrofuran / 24 h / 40 °C
2: dihydrogen peroxide / tetrahydrofuran; acetic acid / 6 h / 25 °C
3: trifluoroacetic acid / dichloromethane / 1 h / 25 °C
4: i-Amyl alcohol / 24 h / Reflux
5: sodium cyanoborohydride / methanol / 1 h / 25 °C
6: hydrogen; palladium 10% on activated carbon / methanol / 45 °C
With
palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; sodium cyanoborohydride; trifluoroacetic acid; potassium hydroxide;
In
tetrahydrofuran; methanol; i-Amyl alcohol; dichloromethane; acetic acid;
DOI:10.1016/j.bmcl.2013.07.071
