Technology Process of 1,2-di-O-octadecyl-sn-glycerol 3-
There total 3 articles about 1,2-di-O-octadecyl-sn-glycerol 3- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Triphenylsilyl chloride;
In
pyridine;
for 3h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) dibutyltin oxide / 1.) benzene, reflux, 1,5 h; 2.) 180-190 deg C, 30 min
2: 90 percent / H2 / 10percent palladium on charcoal / ethanol; acetic acid / 45 °C / 760 Torr
3: 55 percent / TPS-Cl / pyridine / 3 h / Ambient temperature
With
Triphenylsilyl chloride; hydrogen; di(n-butyl)tin oxide;
palladium on activated charcoal;
In
pyridine; ethanol; acetic acid;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 90 percent / H2 / 10percent palladium on charcoal / ethanol; acetic acid / 45 °C / 760 Torr
2: 55 percent / TPS-Cl / pyridine / 3 h / Ambient temperature
With
Triphenylsilyl chloride; hydrogen;
palladium on activated charcoal;
In
pyridine; ethanol; acetic acid;
