Technology Process of C23H24N4O4
There total 5 articles about C23H24N4O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 4 steps
1.1: 4-Nitrophenyl chloroformate; pyridine / dichloromethane / 18 h
1.2: 3 h / Reflux
2.1: lithium hydroxide; water / methanol; tetrahydrofuran
2.2: 18 h
2.3: 3 h
3.1: lithium hydroxide; water / tetrahydrofuran
3.2: 18 h
4.1: sodium carbonate / N,N-dimethyl-formamide; water / 60 °C
With
pyridine; water; sodium carbonate; 4-Nitrophenyl chloroformate; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.04.002
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hydroxide; water / tetrahydrofuran
1.2: 18 h
2.1: sodium carbonate / N,N-dimethyl-formamide; water / 60 °C
With
water; sodium carbonate; lithium hydroxide;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.04.002