(+/-)-N_b-benzyl suaveoline

Base Information

• Chemical Name: (+/-)-N_b-benzyl suaveoline
• CAS No.: 122490-91-9
• Molecular Formula: C₂₇H₂₇N₃
• Molecular Weight: 393.531

Synonyms:

Chemical Property of (+/-)-N_b-benzyl suaveoline

Chemical Property:

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Technology Process of (+/-)-N_b-benzyl suaveoline

There total 8 articles about (+/-)-N_b-benzyl suaveoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

α-ethyl-5-methyl-9-hydroxymethyl-12-benzyl-6,7,8,9,10,11-hexahydro-6,10-imino-5H-cyclooctindole-8-acetaldehyde ethylene acetal (122490-88-4,122490-97-5) → (+/-)-Nb-benzyl suaveoline (122490-91-9,143120-75-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 53 percent / benzeneseleninic anhydride / chlorobenzene / 0.25 h / 110 °C

2: 91 percent / 2N HCl / tetrahydrofuran / 24 h / 25 °C

3: NH₂OH*HCl / ethanol / 16 h / Heating

With hydrogenchloride; benzeneseleninic anhydride; hydroxylamine hydrochloride; In tetrahydrofuran; ethanol; chlorobenzene;

DOI:10.1016/S0040-4020(01)88507-0

Reference yield:

C27H30N2O3 (122490-90-8,141977-81-3) → (+/-)-Nb-benzyl suaveoline (122490-91-9,143120-75-6)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; for 16h; Yield given; Heating;

DOI:10.1021/ja00201a034 DOI:10.1016/S0040-4020(01)88507-0

Reference yield:

α-Ethyl-5-methyl-9-formyl-12-benzyl-6,7,8,9,10,11-hexahydro-6,10-imino-5H-cyclooctindole-8-acetaldehyde ethylene acetal Nb-oxide (122490-89-5,141816-69-5) → (+/-)-Nb-benzyl suaveoline (122490-91-9,143120-75-6)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl / tetrahydrofuran / 24 h / 25 °C

2: NH₂OH*HCl / ethanol / 16 h / Heating

With hydrogenchloride; hydroxylamine hydrochloride; In tetrahydrofuran; ethanol;

DOI:10.1021/ja00201a034

upstream raw materials:

C₂₇H₃₀N₂O₃

α-ethyl-5-methyl-9-hydroxymethyl-12-benzyl-6,7,8,9,10,11-hexahydro-6,10-imino-5H-cyclooctindole-8-acetaldehyde ethylene acetal

α-ethyl-5-methyl-9-methylene-12-benzyl-6,7,8,9,10,11-hexahydro-6,10-imino-5H-cyclooctindole-8-ethanol

α-ethyl-5-methyl-9-methylene-12-benzyl-6,7,8,9,10,11-hexahydro-6,10-imino-5H-cyclooctindole-8-acetaldehyde

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