Technology Process of C20H24N2O3S
There total 7 articles about C20H24N2O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / water; dichloromethane / 20 °C
2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 20 °C
3.1: diisobutylaluminium hydride / toluene / 4 h / 50 °C
3.2: 24 h / 110 °C
4.1: palladium; formic acid / 24 h / 20 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; formic acid; diisobutylaluminium hydride; benzotriazol-1-ol; palladium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1016/j.bmcl.2014.06.014
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 20 °C
2.1: diisobutylaluminium hydride / toluene / 4 h / 50 °C
2.2: 24 h / 110 °C
3.1: palladium; formic acid / 24 h / 20 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; formic acid; diisobutylaluminium hydride; palladium;
In
tetrahydrofuran; toluene;
DOI:10.1016/j.bmcl.2014.06.014
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tert.-butyl lithium / pentane; tetrahydrofuran / 1.5 h / -70 - -30 °C
1.2: -70 °C
2.1: (1R,2S)-1-Amino-2-indanol; borane / tetrahydrofuran / 0.25 h / 20 °C
3.1: potassium carbonate / acetone; water / 24 h / 50 °C
4.1: diisobutylaluminium hydride / toluene / 4 h / 50 °C
4.2: 24 h / 110 °C
5.1: palladium; formic acid / 24 h / 20 °C
With
formic acid; (1R,2S)-1-Amino-2-indanol; borane; tert.-butyl lithium; diisobutylaluminium hydride; potassium carbonate; palladium;
In
tetrahydrofuran; water; acetone; toluene; pentane;
1.2: |Weinreb Ketone Synthesis / 2.1: |Corey-Bakshi-Shibata Reduction;
DOI:10.1016/j.bmcl.2014.06.014