Triphenyl(5,6,7,8-tetrahydro-3-methyl-4H-cycloheptisoxazol-8-yl)phosphonium-chlorid

Base Information

Chemical Name:Triphenyl(5,6,7,8-tetrahydro-3-methyl-4H-cycloheptisoxazol-8-yl)phosphonium-chlorid
CAS No.:75624-82-7
Molecular Formula:C₂₇H₂₇NOP*Cl
Molecular Weight:447.944
Hs Code.:

Triphenyl(5,6,7,8-tetrahydro-3-methyl-4H-cyclohept<d>isoxazol-8-yl)phosphonium-chlorid

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Triphenyl(5,6,7,8-tetrahydro-3-methyl-4H-cycloheptisoxazol-8-yl)phosphonium-chlorid

Chemical Property:

Purity/Quality:

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Technology Process of Triphenyl(5,6,7,8-tetrahydro-3-methyl-4H-cycloheptisoxazol-8-yl)phosphonium-chlorid

There total 3 articles about Triphenyl(5,6,7,8-tetrahydro-3-methyl-4H-cycloheptisoxazol-8-yl)phosphonium-chlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (3-Acetyl-2-oxocycloheptyl)triphenylphosphonium-chlorid

: 75624-82-7
Triphenyl(5,6,7,8-tetrahydro-3-methyl-4H-cycloheptisoxazol-8-yl)phosphonium-chlorid

Guidance literature:: With hydroxylamine hydrochloride; In water; for 8h; Yield given; Heating;

Reference yield:

: 1-<2-Methoxy-3-(triphenylphosphoranyliden)-1-cyclohepten-1-yl>ethanon

: 75624-82-7
Triphenyl(5,6,7,8-tetrahydro-3-methyl-4H-cycloheptisoxazol-8-yl)phosphonium-chlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 2 N HCl / 5 h / Heating

2: NH₂OH*HCl / H₂O / 8 h / Heating

With hydrogenchloride; hydroxylamine hydrochloride; In water;

Reference yield:

: 74581-97-8
2-(Methoxy-1-cyclohepten-1-yl)triphenylphosphonium-bromid

: 75624-82-7
Triphenyl(5,6,7,8-tetrahydro-3-methyl-4H-cycloheptisoxazol-8-yl)phosphonium-chlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, hexane, -30 to -25 deg C, 90 min, 2.) THF, -30 to -25 deg C, 2 h

2: 2 N HCl / 5 h / Heating

3: NH₂OH*HCl / H₂O / 8 h / Heating

With hydrogenchloride; n-butyllithium; hydroxylamine hydrochloride; In water;