dibutyl(ethylthio)stannyl ethyl 4-methoxyphenylphosphonotrithioate

Base Information

• Chemical Name: dibutyl(ethylthio)stannyl ethyl 4-methoxyphenylphosphonotrithioate
• CAS No.: 369645-45-4
• Molecular Formula: C₁₉H₃₅OPS₄Sn
• Molecular Weight: 557.434
• Mol file: 369645-45-4.mol

Synonyms:

Chemical Property of dibutyl(ethylthio)stannyl ethyl 4-methoxyphenylphosphonotrithioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dibutyl(ethylthio)stannyl ethyl 4-methoxyphenylphosphonotrithioate

There total 1 articles about dibutyl(ethylthio)stannyl ethyl 4-methoxyphenylphosphonotrithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

Lawessons reagent (19172-47-5,94367-93-8) + dibutylbis(ethylthio)stannane (13371-37-4) → dibutyl(ethylthio)stannyl ethyl 4-methoxyphenylphosphonotrithioate (369645-45-4)

Guidance literature:

In benzene; Lawesson's reagent added by portions to a soln. of Sn deriv. in dry C6H6at 10°C under Ar with stirring; stirred for 4 h at 10°C; filtered, filtrate evacuated at 0.5 and 0.04 mm Hg for 2 h at 40°C; film distillation; elem. anal.;

DOI:10.1023/A:1012393115659

upstream raw materials:

Lawessons reagent

dibutylbis(ethylthio)stannane

Refernces