(E)-11-(3-propylidene)-6,11-dihydrodibenzothiepin

Base Information

• Chemical Name: (E)-11-(3-propylidene)-6,11-dihydrodibenzothiepin
• CAS No.: 85196-04-9
• Molecular Formula: C₃₁H₄₃NO₂S
• Molecular Weight: 493.754
• Mol file: 85196-04-9.mol

Synonyms:

Chemical Property of (E)-11-(3-propylidene)-6,11-dihydrodibenzothiepin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-11-(3-propylidene)-6,11-dihydrodibenzothiepin

There total 2 articles about (E)-11-(3-propylidene)-6,11-dihydrodibenzothiepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Northiadene (24881-71-8) → (E)-11-(3-propylidene)-6,11-dihydrodibenzothiepin (85196-04-9,344758-26-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / Na₂CO₃ / dimethylformamide

2: CHCl₃

With sodium carbonate; In chloroform; N,N-dimethyl-formamide;

DOI:10.1135/cccc19830163

Reference yield:

(E)-11-(3-propylidene)-6,11-dihydrodibenzothiepin (85196-00-5) + n-decanoyl chloride (112-13-0) → (E)-11-(3-propylidene)-6,11-dihydrodibenzothiepin (85196-04-9,344758-26-5)

Guidance literature:

In chloroform; Yield given;

DOI:10.1135/cccc19830163

upstream raw materials:

(E)-11-(3-propylidene)-6,11-dihydrodibenzothiepin

n-decanoyl chloride

Northiadene