C₁₆H₁₆F₃NO₂

Base Information

Chemical Name:C₁₆H₁₆F₃NO₂
CAS No.:1316312-30-7
Molecular Formula:C₁₆H₁₆F₃NO₂
Molecular Weight:311.304
Hs Code.:

C<sub>16</sub>H<sub>16</sub>F<sub>3</sub>NO<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₆F₃NO₂

Chemical Property:

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Technology Process of C₁₆H₁₆F₃NO₂

There total 4 articles about C₁₆H₁₆F₃NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₈F₃NO₃

: 1316312-30-7
C₁₆H₁₆F₃NO₂

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; triethylamine; In dichloromethane; at 70 ℃; for 72h; Inert atmosphere;
DOI:10.3762/bjoc.7.108

Reference yield:

: 211230-12-5
(S)-3-phenylbutyronitrile

: 1316312-30-7
C₁₆H₁₆F₃NO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / diethyl ether; hexane / -40 °C / Inert atmosphere

1.2: Inert atmosphere; Cooling

1.3: 20 °C / Inert atmosphere; Cooling

2.1: trimethylsilyl trifluoromethanesulfonate; triethylamine / dichloromethane / 72 h / 70 °C / Inert atmosphere

With n-butyllithium; trimethylsilyl trifluoromethanesulfonate; triethylamine; In diethyl ether; hexane; dichloromethane;
DOI:10.3762/bjoc.7.108

Reference yield:

: (S)-3-phenylbutyramide

: 1316312-30-7
C₁₆H₁₆F₃NO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,3,5-trichloro-2,4,6-triazine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / diethyl ether; hexane / -40 °C / Inert atmosphere

2.2: Inert atmosphere; Cooling

2.3: 20 °C / Inert atmosphere; Cooling

3.1: trimethylsilyl trifluoromethanesulfonate; triethylamine / dichloromethane / 72 h / 70 °C / Inert atmosphere

With n-butyllithium; 1,3,5-trichloro-2,4,6-triazine; trimethylsilyl trifluoromethanesulfonate; triethylamine; In diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3762/bjoc.7.108