[(1,1,1-tris((diethylphosphino)methyl)ethane)Fe(μ-Cl)3Fe(1,1,1-tris((diethylphosphino)methyl)ethane)] tetraphenylborate*methylene chloride

Base Information

Chemical Name:[(1,1,1-tris((diethylphosphino)methyl)ethane)Fe(μ-Cl)3Fe(1,1,1-tris((diethylphosphino)methyl)ethane)] tetraphenylborate*methylene chloride
CAS No.:79682-20-5
Molecular Formula:CH₂Cl₂*C₂₄H₂₀B*C₃₄H₇₈Cl₃Fe₂P₆
Molecular Weight:1295.06
Hs Code.:

[(1,1,1-tris((diethylphosphino)methyl)ethane)Fe(μ-Cl)3Fe(1,1,1-tris((diethylphosphino)methyl)ethane)] tetraphenylborate*methylene chloride

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Suppliers and Price of [(1,1,1-tris((diethylphosphino)methyl)ethane)Fe(μ-Cl)3Fe(1,1,1-tris((diethylphosphino)methyl)ethane)] tetraphenylborate*methylene chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [(1,1,1-tris((diethylphosphino)methyl)ethane)Fe(μ-Cl)3Fe(1,1,1-tris((diethylphosphino)methyl)ethane)] tetraphenylborate*methylene chloride

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Technology Process of [(1,1,1-tris((diethylphosphino)methyl)ethane)Fe(μ-Cl)3Fe(1,1,1-tris((diethylphosphino)methyl)ethane)] tetraphenylborate*methylene chloride

There total 1 articles about [(1,1,1-tris((diethylphosphino)methyl)ethane)Fe(μ-Cl)3Fe(1,1,1-tris((diethylphosphino)methyl)ethane)] tetraphenylborate*methylene chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: iron(II) chloride hexahydrate

: 22031-14-7
1,1,1-tris(diethylphosphinomethyl)ethane

: 143-66-8
sodium tetraphenyl borate

: 79682-20-5
[(1,1,1-tris((diethylphosphino)methyl)ethane)Fe(μ-Cl)3Fe(1,1,1-tris((diethylphosphino)methyl)ethane)] tetraphenylborate*methylene chloride

Guidance literature:: With CH₂Cl₂; In ethanol; dichloromethane; under N2 etriphos/CH2Cl2 added at room temp. to Fe-complex/EtOH, NaBPh4added, stirred; n-Bu2O added, evapn., cryst. washed (EtOH/n-Bu2O, petroleum ether), recrystd. (petroleum ether), elem. anal.;