1,6-dithiocyanato-1,3,5-cycloheptatriene

Base Information

Chemical Name:1,6-dithiocyanato-1,3,5-cycloheptatriene
CAS No.:78638-65-0
Molecular Formula:C₉H₆N₂S₂
Molecular Weight:206.292
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-dithiocyanato-1,3,5-cycloheptatriene

Chemical Property:

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Technology Process of 1,6-dithiocyanato-1,3,5-cycloheptatriene

There total 1 articles about 1,6-dithiocyanato-1,3,5-cycloheptatriene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 505-14-6
thiocyanogen

: 4646-69-9
benzocyclopropene

: 78638-65-0
1,6-dithiocyanato-1,3,5-cycloheptatriene

: 78672-48-7
o-thiocyanatobenzyl isothiocyanate

: 78638-66-1
o-thiocyanatobenzyl thiocyanate

Guidance literature:: In benzene; for 0.5h; Ambient temperature; Irradiation;
DOI:10.1021/jo00202a008

Reference yield:

: 78638-65-0
1,6-dithiocyanato-1,3,5-cycloheptatriene

: 94042-23-6
C₁₉H₁₅NO₂S₂

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium, liquid NH₃ / 1.) -78 deg C, 2.) THF, HMPA, RT, 5 h

2: 59 percent / xylene / 2 h / Heating

With ammonia; sodium; In xylene;
DOI:10.1021/jo00202a008

Reference yield:

: 78638-65-0
1,6-dithiocyanato-1,3,5-cycloheptatriene

: 94042-22-5
C₁₉H₁₇NO₂S₂

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium, liquid NH₃ / 1.) -78 deg C, 2.) THF, HMPA, RT, 1 h

2: 77 percent / xylene / 96 h / Heating

With ammonia; sodium; In xylene;
DOI:10.1021/jo00202a008