V(CN(CH₃)2C₆H₃)4(CO)2

Base Information

Chemical Name:V(CN(CH₃)2C₆H₃)4(CO)2
CAS No.:272456-51-6
Molecular Formula:C₃₈H₃₆N₄O₂V
Molecular Weight:631.671
Hs Code.:

V(CN(CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4(CO)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of V(CN(CH₃)2C₆H₃)4(CO)2

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Technology Process of V(CN(CH₃)2C₆H₃)4(CO)2

There total 1 articles about V(CN(CH₃)2C₆H₃)4(CO)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 14024-00-1
vanadium hexacarbonyl

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 272456-51-6,272778-09-3
V(CN(CH₃)2C₆H₃)4(CO)2

Guidance literature:: In n-heptane; soln. of V(CO)6 in heptane was added to soln. of ligand in heptane at room temp., 7 h, mixt. was stirred for 72 h at room temp. under Ar; solvent was removed in vacuo, filtered, washed with pentane, dried undervac., redissolved in toluene, filtered, solvent was removed, recrystd. from THF/pentane; elem. anal.;
DOI:10.1021/ja000212w

Reference yield: 80.0%

: ferrocenium hexafluorophosphate

: 272456-51-6,272778-09-3
V(CN(CH₃)2C₆H₃)4(CO)2

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 200487-87-2
V(CN(CH₃)2C₆H₃)6⁽¹⁺⁾*PF₆^(1-)=V(CN(CH₃)2C₆H₃)6PF₆

Guidance literature:: In tetrahydrofuran; soln. of V-complex and ligand in THF was transferred to suspn. of Fe-complex in THF at 0°C, mixt. was stirred for 15 h, warmed to room temp. under Ar; filtered, concd., heptane was added, filtered off, washed with pentane, dried under vac.;
DOI:10.1021/ja000212w