13-cis-14-methylretinal

Base Information

Chemical Name:13-cis-14-methylretinal
CAS No.:53153-16-5
Molecular Formula:C₂₁H₃₀O
Molecular Weight:298.469
Hs Code.:

Synonyms:

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Chemical Property of 13-cis-14-methylretinal

Chemical Property:

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Technology Process of 13-cis-14-methylretinal

There total 6 articles about 13-cis-14-methylretinal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59057-30-6
(1E)-1-(2,6,6-trimethylcyclohex-1-enyl)-3-methyl-1,4-pentadien-3-ol

: 53153-16-5
13-cis-14-methylretinal

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / 36percent HCl / methanol / 5 h / Ambient temperature

2: 1.) 30percent NaOMe 2.) 10percent H₂SO₄ / 1.) DMF, 2 h, -10 deg C to -20 deg C, 3.5h, 50 deg C; 2.) 9 h

With hydrogenchloride; sulfuric acid; sodium methylate; In methanol;

Reference yield:

: 103410-80-6
(E)-4,4-Dimethoxy-2,3-dimethyl-2-butenol

: 53153-16-5
13-cis-14-methylretinal

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / MnO₂ / acetone / 19 h / Ambient temperature

2: 1.) 30percent NaOMe 2.) 10percent H₂SO₄ / 1.) DMF, 2 h, -10 deg C to -20 deg C, 3.5h, 50 deg C; 2.) 9 h

With manganese(IV) oxide; sulfuric acid; sodium methylate; In acetone;

Reference yield:

: 103410-79-3
(E)-4,4-Dimethoxy-2,3-dimethyl-2-butensaeure-ethylester

: 53153-16-5
13-cis-14-methylretinal

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / LiAlH₄ / diethyl ether / 0.12 h / 0 °C

2: 90 percent / MnO₂ / acetone / 19 h / Ambient temperature

3: 1.) 30percent NaOMe 2.) 10percent H₂SO₄ / 1.) DMF, 2 h, -10 deg C to -20 deg C, 3.5h, 50 deg C; 2.) 9 h

With manganese(IV) oxide; lithium aluminium tetrahydride; sulfuric acid; sodium methylate; In diethyl ether; acetone;