Technology Process of C22H36O5Si
There total 13 articles about C22H36O5Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrahydrofuran / 0.5 h / 20 °C
2: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C
With
dihydrogen peroxide; sodium hydroxide;
In
tetrahydrofuran; water;
DOI:10.1021/ja305864z
- Guidance literature:
-
With
dihydrogen peroxide; sodium hydroxide;
In
tetrahydrofuran; water;
at 0 - 20 ℃;
for 2h;
DOI:10.1021/ja305864z
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: camphor-10-sulfonic acid / methanol; dichloromethane / 5 h / 0 °C
2.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C
3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C
3.2: 2 h / -78 - 0 °C
4.1: tetrahydrofuran / 0.5 h / 20 °C
5.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C
With
camphor-10-sulfonic acid; potassium tert-butylate; dihydrogen peroxide; sulfur trioxide pyridine complex; triethylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/ja305864z