2-Amino-4-iodobenzoic acid

Base Information

• Chemical Name: 2-Amino-4-iodobenzoic acid
• CAS No.: 20776-54-9
• Molecular Formula: C7H6INO2
• Molecular Weight: 263.035
• Hs Code.: 2922499990
• Mol file: 20776-54-9.mol

Synonyms:2-AMINO-4-IODOBENZOIC ACID

Chemical Property of 2-Amino-4-iodobenzoic acid

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 208 °C (decomp)(Solv: ethanol (64-17-5))
• Refractive Index: 1.728
• Boiling Point: 377.02 °C at 760 mmHg
• PKA: 4.76±0.10(Predicted)
• Flash Point: 181.815 °C
• PSA: 63.32000
• Density: 2.082 g/cm³
• LogP: 2.15280
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

2-Amino-4-iodobenzoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Amino-4-iodobenzoic acid

There total 6 articles about 2-Amino-4-iodobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-iodo-2-nitro benzoic acid (116529-62-5) → 2-amino-4-iodobenzoic acid (20776-54-9)

Guidance literature:

With tin(ll) chloride; In ethyl acetate; at 20 ℃; for 16h;

Reference yield: 84.0%

6-iodoisatin (20780-77-2) → 2-amino-4-iodobenzoic acid (20776-54-9)

Guidance literature:

With sodium hydroxide; dihydrogen peroxide; at 50 ℃;

DOI:10.1016/j.bmc.2008.07.015

Reference yield: 80.0%

4-iodo-2-nitrotoluene (41252-97-5) → 2-amino-4-iodobenzoic acid (20776-54-9)

Guidance literature:

With selenium; nitrobenzene; sodium hydroxide; In methanol; water; dimethyl sulfoxide; at 90 ℃; for 5h; Inert atmosphere;

DOI:10.1039/d0gc04407e

upstream raw materials:

6-iodoisatin

4-iodo-2-nitro benzoic acid

anthranilic acid

2-amino-4-bromobenzoic acid

Downstream raw materials:

2-amino-4,5-diiodo-benzoic acid

7-iodo-2-(2-methoxy-phenoxymethyl)-benzo[d][1,3]oxazin-4-one

5-Iod-benzoldiazonium-2-carboxylat

3,4-diiodobenzoic acid