1-benzyl-2-phenyl-3-ethoxycarbonylquinoxaline<2,3e>benzindole

Base Information

• Chemical Name: 1-benzyl-2-phenyl-3-ethoxycarbonylquinoxaline<2,3e>benzindole
• CAS No.: 123647-47-2
• Molecular Formula: C₃₄H₂₅N₃O₂
• Molecular Weight: 507.591
• Mol file: 123647-47-2.mol

Synonyms:

Chemical Property of 1-benzyl-2-phenyl-3-ethoxycarbonylquinoxaline<2,3e>benzindole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-benzyl-2-phenyl-3-ethoxycarbonylquinoxaline<2,3e>benzindole

There total 4 articles about 1-benzyl-2-phenyl-3-ethoxycarbonylquinoxaline<2,3e>benzindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

ethyl ester of 1-benzyl-4,5-dioxo-2-phenylbenzindole-3-carboxylic acid (115979-13-0) + 1,2-diamino-benzene (95-54-5) → 1-benzyl-2-phenyl-3-ethoxycarbonylquinoxaline<2,3e>benzindole (123647-47-2)

Guidance literature:

In acetic acid; for 0.0833333h; Heating;

DOI:10.1007/BF00472619

Reference yield:

2,3-Dichloro-1,4-naphthoquinone (117-80-6) → 1-benzyl-2-phenyl-3-ethoxycarbonylquinoxaline<2,3e>benzindole (123647-47-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 36 percent / CH₃COONa / ethanol / 2 h / Heating

2: 60 percent / CH₃COONa / acetic acid / 1 h / Heating

3: 98 percent / acetic acid / 0.08 h / Heating

With sodium acetate; In ethanol; acetic acid;

DOI:10.1007/BF00472619

Reference yield:

ethyl (2Z)-3-(benzylamino)-3-phenylacrylate (14191-09-4,73148-43-3) → 1-benzyl-2-phenyl-3-ethoxycarbonylquinoxaline<2,3e>benzindole (123647-47-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 36 percent / CH₃COONa / ethanol / 2 h / Heating

2: 60 percent / CH₃COONa / acetic acid / 1 h / Heating

3: 98 percent / acetic acid / 0.08 h / Heating

With sodium acetate; In ethanol; acetic acid;

DOI:10.1007/BF00472619

upstream raw materials:

ethyl ester of 1-benzyl-4,5-dioxo-2-phenylbenzindole-3-carboxylic acid

1,2-diamino-benzene

2,3-Dichloro-1,4-naphthoquinone

ethyl (2Z)-3-(benzylamino)-3-phenylacrylate