S-(2-CYANO-2-PROPYL)-S-DODECYLTRITHIOCARBONATE

Base Information

• Chemical Name: S-(2-CYANO-2-PROPYL)-S-DODECYLTRITHIOCARBONATE
• CAS No.: 870196-83-1
• Molecular Formula: C17H31NS3
• Molecular Weight: 345.638
• Hs Code.: 2930909899
• Mol file: 870196-83-1.mol

Synonyms:S-(2-Cyanoprop-2-yl)-S-dodecyltrithiocarbonate;2-Cyano-2-propyl dodecyl trithiocarbonate;

Chemical Property of S-(2-CYANO-2-PROPYL)-S-DODECYLTRITHIOCARBONATE

Chemical Property:

• Refractive Index: n20/D1.535
• Boiling Point: 476.9±24.0 °C(Predicted)
• Flash Point: >110℃
• PSA: 106.48000
• Density: 0.991 g/mL at 25 °C
• LogP: 6.96078
• Storage Temp.: 2-8°C
• Sensitive.: light sensitive, store cold

Purity/Quality:

98%, ^*data from raw suppliers

2-Cyano-2-propyl Dodecyl Trithiocarbonate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Uses: Sulfur-based agent providing a high degree of control for, Reversible Addition Fragmentation Chain Transfer (RAFT), Reversible Addition Fragmentation Chain Transfer (RAFT) Polymerization

Technology Process of S-(2-CYANO-2-PROPYL)-S-DODECYLTRITHIOCARBONATE

There total 1 articles about S-(2-CYANO-2-PROPYL)-S-DODECYLTRITHIOCARBONATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2,2'-azobis(isobutyronitrile) (78-67-1) + S,S'-bis(1-dodecyl)trithiocarbonate (1608-90-8) → S-dodecyl-S'-[dimethylcyanomethyl]trithiocarbonate (870196-83-1)

Guidance literature:

2,2'-azobis(isobutyronitrile); S,S'-bis(1-dodecyl)trithiocarbonate; In ethyl acetate; for 0.666667h; Inert atmosphere;

In ethyl acetate; at 77 ℃; for 12h; Inert atmosphere;

DOI:10.1021/acs.macromol.5b02463

Reference yield: 16.0%

N-benzylmethacrylamide (3219-55-4) + S-dodecyl-S'-[dimethylcyanomethyl]trithiocarbonate (870196-83-1) → C28H44N2OS3

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In N,N-dimethyl-formamide; at 60 ℃; for 24h; Inert atmosphere;

DOI:10.1021/acs.macromol.5b02463

Reference yield: 10.0%

S-dodecyl-S'-[dimethylcyanomethyl]trithiocarbonate (870196-83-1) + 2-methyl-N-phenylacrylamide (1611-83-2) → C27H42N2OS3

Guidance literature:

With 2,2’-azobis(4-methoxy-2,4-dimethyl)valeronitrile; In N,N-dimethyl-formamide; at 30 ℃; for 48h; Inert atmosphere;

DOI:10.1021/acs.macromol.5b02463

upstream raw materials:

2,2'-azobis(isobutyronitrile)

S,S'-bis(1-dodecyl)trithiocarbonate

Downstream raw materials:

1-dodecylthiol

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