1,1μ-Bis(di-cyclohexylphosphino)ferrocene palladium dichloride

Base Information

• Chemical Name: 1,1μ-Bis(di-cyclohexylphosphino)ferrocene palladium dichloride
• CAS No.: 917511-90-1
• Molecular Formula: C₃₄H₅₂Cl₂FeP₂Pd
• Molecular Weight: 755.907
• Mol file: 917511-90-1.mol

Synonyms:[PdCl2(1,1'-bis(dicyclohexylphosphino)ferrocene)];2,5-Ala-enkephalinamide;Dichloro[1,1'-bis(dicyclohexylphosphino)ferrocene]palladium(II),dichloromethane adduct;<D-AlaL2,L-AlaL5>enkephalinamide;[Pd(dcpf)Cl2];Enkephalinamide,alanine(2,5);PdCl2(dcpf);(DCPF)PdCl2;Enkephalinamide,ala(2,5);查看更多英文别名收起

Chemical Property of 1,1μ-Bis(di-cyclohexylphosphino)ferrocene palladium dichloride

Chemical Property:

• Melting Point: 294-300ºC
• PSA: 27.18000
• LogP: 11.79670
• Storage Temp.: ?20°C

Purity/Quality:

99%, ^*data from raw suppliers

Dichloro[1,1'-bis(dicyclohexylphosphino)ferrocene]palladium(II), dichloromethane adduct, 99% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Uses: 1,1'-Bis(di-cyclohexylphosphino)ferrocene palladium dichloride is an air-stable catalyst useful in the arylation of various ketones with aryl chlorides and aryl bromides. 1,1′-Bis(di-cyclohexylphosphino)ferrocene]dichloropalladium(II) or (Pd(dcpf)Cl2) can be used as a catalyst in the synthesis of: α, β-unsaturated amides by hydroaminocarbonylation of alkynes with tertiary amines.Quinazoline derivatives via Suzuki-Miyaura coupling reaction between of quinazolines containing unprotected NH2 group and arylboronic acids. α-aryl carbonyl compounds by α-arylation of ketones with aryl chlorides and aryl bromides.

Technology Process of 1,1μ-Bis(di-cyclohexylphosphino)ferrocene palladium dichloride

There total 1 articles about 1,1μ-Bis(di-cyclohexylphosphino)ferrocene palladium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

bis(benzonitrile)palladium(II) dichloride (15617-18-2,39958-10-6,14220-64-5) + 1,1'-bis(dicyclohexylphosphinocyclopentadienyl)iron (146960-90-9) → [1,1′-bis(di-cyclohexylphosphino)ferrocene]dichloropalladium (II) (917511-90-1)

Guidance literature:

In dichloromethane; Ar atm., Schlenk techniques; 1,1'-bis(dicyclohexylphosphino)ferrocene and PdCl2(PhCN)2 in CH2Cl2 stirred for 2 h; addn. of Et2O, mixt. stirred for 5 min, filtration, filtrate concd. and layered with Et2O, crystn. on cooling in freezer; elem. anal.;

DOI:10.1016/j.jorganchem.2006.08.030

upstream raw materials:

bis(benzonitrile)palladium(II) dichloride

1,1'-bis(dicyclohexylphosphinocyclopentadienyl)iron

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