(ethoxycarbonyl-4 methyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2 o-methoxycarbonylbenzamido-2 ethanoate de tert-butyle

Base Information

• Chemical Name: (ethoxycarbonyl-4 methyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2 o-methoxycarbonylbenzamido-2 ethanoate de tert-butyle
• CAS No.: 115817-91-9
• Molecular Formula: C₂₄H₃₀N₂O₈S
• Molecular Weight: 506.577
• Mol file: 115817-91-9.mol

Synonyms:

Chemical Property of (ethoxycarbonyl-4 methyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2 o-methoxycarbonylbenzamido-2 ethanoate de tert-butyle

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (ethoxycarbonyl-4 methyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2 o-methoxycarbonylbenzamido-2 ethanoate de tert-butyle

There total 1 articles about (ethoxycarbonyl-4 methyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2 o-methoxycarbonylbenzamido-2 ethanoate de tert-butyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-[1-tert-Butoxycarbonyl-1-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-meth-(Z)-ylidene]-5-methyl-3,6-dihydro-2H-[1,3]thiazine-4-carboxylic acid ethyl ester (121534-76-7) → (ethoxycarbonyl-4 methyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2 o-methoxycarbonylbenzamido-2 ethanoate de tert-butyle (115817-91-9)

Guidance literature:

DOI:10.1016/S0040-4020(01)85101-2

Reference yield:

(ethoxycarbonyl-4 methyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2 o-methoxycarbonylbenzamido-2 ethanoate de tert-butyle (115817-91-9) → 2-[tert-Butoxycarbonyl-methoxy-(2-methoxycarbonyl-benzoylamino)-methyl]-5-methyl-3,6-dihydro-2H-[1,3]thiazine-4-carboxylic acid ethyl ester (115818-00-3,115818-02-5)

Guidance literature:

With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; Ambient temperature;

DOI:10.1016/S0040-4020(01)85101-2

upstream raw materials:

2-[1-tert-Butoxycarbonyl-1-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-meth-(Z)-ylidene]-5-methyl-3,6-dihydro-2H-[1,3]thiazine-4-carboxylic acid ethyl ester

Downstream raw materials:

2-[tert-Butoxycarbonyl-methoxy-(2-methoxycarbonyl-benzoylamino)-methyl]-5-methyl-3,6-dihydro-2H-[1,3]thiazine-4-carboxylic acid ethyl ester