trans-<4α(S*),6α,8α,9aα>-(+/-)-octahydro-6-(3-iodo-4-methoxyphenyl)-α-<2-(3-iodo-4-methoxyphenyl)ethenyl>-8-(phenylmethoxy)-2H-quinolizine-4-ethanol

Base Information

Chemical Name:trans-<4α(S*),6α,8α,9aα>-(+/-)-octahydro-6-(3-iodo-4-methoxyphenyl)-α-<2-(3-iodo-4-methoxyphenyl)ethenyl>-8-(phenylmethoxy)-2H-quinolizine-4-ethanol
CAS No.:97974-80-6
Molecular Formula:C₃₄H₃₉I₂NO₄
Molecular Weight:779.497
Hs Code.:

trans-<4α(S*),6α,8α,9aα>-(+/-)-octahydro-6-(3-iodo-4-methoxyphenyl)-α-<2-(3-iodo-4-methoxyphenyl)ethenyl>-8-(phenylmethoxy)-2H-quinolizine-4-ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-<4α(S*),6α,8α,9aα>-(+/-)-octahydro-6-(3-iodo-4-methoxyphenyl)-α-<2-(3-iodo-4-methoxyphenyl)ethenyl>-8-(phenylmethoxy)-2H-quinolizine-4-ethanol

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Technology Process of trans-<4α(S*),6α,8α,9aα>-(+/-)-octahydro-6-(3-iodo-4-methoxyphenyl)-α-<2-(3-iodo-4-methoxyphenyl)ethenyl>-8-(phenylmethoxy)-2H-quinolizine-4-ethanol

There total 20 articles about trans-<4α(S*),6α,8α,9aα>-(+/-)-octahydro-6-(3-iodo-4-methoxyphenyl)-α-<2-(3-iodo-4-methoxyphenyl)ethenyl>-8-(phenylmethoxy)-2H-quinolizine-4-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 97974-79-3,110454-04-1
trans-(4α,6α,8α,9aα)-(+/-)-4--1-(3-iodo-4-methoxyphenyl)-1-buten-3-one

: 97974-80-6,97974-81-7,110454-05-2,110454-06-3
trans-<4α(R*),6α,8α,9aα>-(+/-)-octahydro-6-(3-iodo-4-methoxyphenyl)-α-<2-(3-iodo-4-methoxyphenyl)ethenyl>-8-(phenylmethoxy)-2H-quinolizine-4-ethanol

: 97974-80-6,97974-81-7,110454-05-2,110454-06-3
trans-<4α(S*),6α,8α,9aα>-(+/-)-octahydro-6-(3-iodo-4-methoxyphenyl)-α-<2-(3-iodo-4-methoxyphenyl)ethenyl>-8-(phenylmethoxy)-2H-quinolizine-4-ethanol

Guidance literature:: With lithium; triethyl-hydrido-borate^(1-);
DOI:10.1021/jo00219a061

Reference yield: 25.0%

: 97974-79-3,110454-04-1
trans-(4α,6α,8α,9aα)-(+/-)-4--1-(3-iodo-4-methoxyphenyl)-1-buten-3-one

: 97974-80-6,97974-81-7,110454-05-2,110454-06-3
trans-<4α(R*),6α,8α,9aα>-(+/-)-octahydro-6-(3-iodo-4-methoxyphenyl)-α-<2-(3-iodo-4-methoxyphenyl)ethenyl>-8-(phenylmethoxy)-2H-quinolizine-4-ethanol

: 97974-80-6,97974-81-7,110454-05-2,110454-06-3
trans-<4α(S*),6α,8α,9aα>-(+/-)-octahydro-6-(3-iodo-4-methoxyphenyl)-α-<2-(3-iodo-4-methoxyphenyl)ethenyl>-8-(phenylmethoxy)-2H-quinolizine-4-ethanol

Guidance literature:: With lithium; triethyl-hydrido-borate^(1-);
DOI:10.1021/jo00219a061

Reference yield:

: 2314-37-6
3-iodo-4-methoxybenzaldehyde

: 97974-80-6,97974-81-7,110454-05-2,110454-06-3
trans-<4α(S*),6α,8α,9aα>-(+/-)-octahydro-6-(3-iodo-4-methoxyphenyl)-α-<2-(3-iodo-4-methoxyphenyl)ethenyl>-8-(phenylmethoxy)-2H-quinolizine-4-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) dimethoxyethane, RT, 1 h, 2.) dimethoxyethane, RT, 6 h

2: 22 percent / lithium triethylborohydride / tetrahydrofuran; CH₂Cl₂ / 0.5 h

With sodium hydride; lithium triethylborohydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00230a003