endo-4a,5,8,8a-tetrahydro-1-hydroxy-1-phenyl-5,8-methanobenzindane-4,9-quinone

Base Information

Chemical Name:endo-4a,5,8,8a-tetrahydro-1-hydroxy-1-phenyl-5,8-methanobenzindane-4,9-quinone
CAS No.:100848-76-8
Molecular Formula:C₂₀H₁₈O₃
Molecular Weight:306.361
Hs Code.:

endo-4a,5,8,8a-tetrahydro-1-hydroxy-1-phenyl-5,8-methanobenz<f>indane-4,9-quinone

Synonyms:

Suppliers and Price of endo-4a,5,8,8a-tetrahydro-1-hydroxy-1-phenyl-5,8-methanobenzindane-4,9-quinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of endo-4a,5,8,8a-tetrahydro-1-hydroxy-1-phenyl-5,8-methanobenzindane-4,9-quinone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of endo-4a,5,8,8a-tetrahydro-1-hydroxy-1-phenyl-5,8-methanobenzindane-4,9-quinone

There total 4 articles about endo-4a,5,8,8a-tetrahydro-1-hydroxy-1-phenyl-5,8-methanobenzindane-4,9-quinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 100848-75-7
1-hydroxy-1-phenylindane-4,7-quinone

: 100848-76-8,100897-78-7
endo-4a,5,8,8a-tetrahydro-1-hydroxy-1-phenyl-5,8-methanobenzindane-4,9-quinone

Guidance literature:: for 1h; Ambient temperature;

Reference yield:

: 52428-09-8
4,7-dimethoxyindan-1-one

: 100848-76-8,100897-78-7
endo-4a,5,8,8a-tetrahydro-1-hydroxy-1-phenyl-5,8-methanobenzindane-4,9-quinone

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / conc HCl / pyridine / 1.5 h / 165 - 170 °C

2: 2.) sodium sulfate, silver oxide / 1.) THf, ether, -75 deg C, 15 min, r.t., 45 min, 2.) r.t., 1 h

3: 100 percent / 1 h / Ambient temperature

With hydrogenchloride; sodium sulfate; silver(l) oxide; In pyridine;

Reference yield:

: 100126-94-1
3-(2,5-dimethoxyphenyl)propionyl chloride

: 100848-76-8,100897-78-7
endo-4a,5,8,8a-tetrahydro-1-hydroxy-1-phenyl-5,8-methanobenzindane-4,9-quinone

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / AlCl₃ / 1,2-dichloro-ethane / 2 h / Ambient temperature

2: 72 percent / conc HCl / pyridine / 1.5 h / 165 - 170 °C

3: 2.) sodium sulfate, silver oxide / 1.) THf, ether, -75 deg C, 15 min, r.t., 45 min, 2.) r.t., 1 h

4: 100 percent / 1 h / Ambient temperature

With hydrogenchloride; aluminium trichloride; sodium sulfate; silver(l) oxide; In pyridine; 1,2-dichloro-ethane;