Boc-D-Ala-ΨPhe-OMe

Base Information

• Chemical Name: Boc-D-Ala-ΨPhe-OMe
• CAS No.: 126027-99-4
• Molecular Formula: C₁₈H₂₆N₂O₄S
• Molecular Weight: 366.481

Synonyms:

Chemical Property of Boc-D-Ala-ΨPhe-OMe

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of Boc-D-Ala-ΨPhe-OMe

There total 1 articles about Boc-D-Ala-ΨPhe-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

N-tert-butyloxycarbonylalanylphenylalanine methyl ester (2280-66-2) → tert-butoxycarbonyl-L-alanylsulfonyl-L-phenylalanine (126027-99-4,142765-11-5)

Guidance literature:

With 2,4-bis(phenylthio)-1,3-dithia-2λ⁵,4λ⁵-diphosphetane 2,4-disulphide; In tetrahydrofuran; Ambient temperature;

Reference yield: 99.0%

tert-butoxycarbonyl-L-alanylsulfonyl-L-phenylalanine (126027-99-4,142765-11-5) → C18H26N2O4(18)O

Guidance literature:

With pyridine; N-chloro-succinimide; ¹⁸O-labeled water; In ethyl acetate; at 20 ℃; for 0.05h; Inert atmosphere;

Reference yield: 70.0%

L-valine allyl ester (88224-01-5) + Boc-D-Ala-ΨPhe-OMe (126027-99-4,142765-11-5) → N-tert-Butyloxycarbonyl-D-thioalanyl-L-phenylalanyl-L-valinallylester (142765-13-7)

Guidance literature:

In water; N,N-dimethyl-formamide; for 48h; chymotrypsin;

upstream raw materials:

N-tert-butyloxycarbonylalanylphenylalanine methyl ester

Downstream raw materials:

Boc-Ala-ψ(CH2NH)-Phe-OMe

(S)-2-((S)-2-Amino-thiopropionylamino)-3-phenyl-propionic acid methyl ester

(S)-2-[(S)-2-((S)-2-tert-Butoxycarbonylamino-propionylamino)-thiopropionylamino]-3-phenyl-propionic acid methyl ester

Boc-D-AlaΨPhe-Leu-NH2

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