Technology Process of 1,6-diphenyl-hexa-1,5-diene
There total 4 articles about 1,6-diphenyl-hexa-1,5-diene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
phosphoric acid;
In
toluene;
for 0.5h;
Overall yield = 4.08 g;
Inert atmosphere;
Reflux;
DOI:10.1002/ejoc.201900528
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium bromide monohydrate / tetrahydrofuran; dibutyl ether / 22 h / 0 °C / Schlenk technique; Inert atmosphere
2: phosphoric acid / toluene / 0.5 h / Inert atmosphere; Reflux
With
lithium bromide monohydrate; phosphoric acid;
In
tetrahydrofuran; dibutyl ether; toluene;
DOI:10.1002/ejoc.201900528
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium bromide monohydrate / tetrahydrofuran; dibutyl ether / 22 h / 0 °C / Schlenk technique; Inert atmosphere
2: phosphoric acid / toluene / 0.5 h / Inert atmosphere; Reflux
With
lithium bromide monohydrate; phosphoric acid;
In
tetrahydrofuran; dibutyl ether; toluene;
DOI:10.1002/ejoc.201900528