{(S)-3-((R)-1-Allyloxycarbonyloxy-ethyl)-2-[2-(4,5-dimethyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-yl)-acetylsulfanyl]-4-oxo-azetidin-1-yl}-(triphenyl-λ⁵-phosphanylidene)-acetic acid allyl ester

Base Information

• Chemical Name: {(S)-3-((R)-1-Allyloxycarbonyloxy-ethyl)-2-[2-(4,5-dimethyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-yl)-acetylsulfanyl]-4-oxo-azetidin-1-yl}-(triphenyl-λ⁵-phosphanylidene)-acetic acid allyl ester
• CAS No.: 133260-74-9
• Molecular Formula: C₄₀H₄₀N₃O₉PS
• Molecular Weight: 769.812

Synonyms:

Chemical Property of {(S)-3-((R)-1-Allyloxycarbonyloxy-ethyl)-2-[2-(4,5-dimethyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-yl)-acetylsulfanyl]-4-oxo-azetidin-1-yl}-(triphenyl-λ⁵-phosphanylidene)-acetic acid allyl ester

Chemical Property:

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Useful:

Technology Process of {(S)-3-((R)-1-Allyloxycarbonyloxy-ethyl)-2-[2-(4,5-dimethyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-yl)-acetylsulfanyl]-4-oxo-azetidin-1-yl}-(triphenyl-λ⁵-phosphanylidene)-acetic acid allyl ester

There total 1 articles about {(S)-3-((R)-1-Allyloxycarbonyloxy-ethyl)-2-[2-(4,5-dimethyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-yl)-acetylsulfanyl]-4-oxo-azetidin-1-yl}-(triphenyl-λ⁵-phosphanylidene)-acetic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4,5-Dimethyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-yl)-acetyl chloride (133260-65-8) + Silver; (S)-3-((R)-1-allyloxycarbonyloxy-ethyl)-1-[allyloxycarbonyl-(triphenyl-λ5-phosphanylidene)-methyl]-4-oxo-azetidine-2-thiolate (104698-13-7) → {(S)-3-((R)-1-Allyloxycarbonyloxy-ethyl)-2-[2-(4,5-dimethyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-yl)-acetylsulfanyl]-4-oxo-azetidin-1-yl}-(triphenyl-λ5-phosphanylidene)-acetic acid allyl ester (133260-74-9)

Guidance literature:

With pyridine; In dichloromethane; Ambient temperature;

DOI:10.3987/COM-88-S101

upstream raw materials:

(4,5-Dimethyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-yl)-acetyl chloride

Silver; (S)-3-((R)-1-allyloxycarbonyloxy-ethyl)-1-[allyloxycarbonyl-(triphenyl-λ⁵-phosphanylidene)-methyl]-4-oxo-azetidine-2-thiolate

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