3-Chloro-4-[(3,4-dichlorophenyl)methoxy]benzenamine

Base Information

• Chemical Name: 3-Chloro-4-[(3,4-dichlorophenyl)methoxy]benzenamine
• CAS No.: 1039922-08-1
• Molecular Formula: C13H10Cl3NO
• Molecular Weight: 302.58
• Mol file: 1039922-08-1.mol

Synonyms:3-Chloro-4-[1,1,2-trifluoro-2-(trifluoromethoxy)ethoxy]benzenamine

Chemical Property of 3-Chloro-4-[(3,4-dichlorophenyl)methoxy]benzenamine

Chemical Property:

• Appearance/Colour: Kind of white to yellow powder
• Boiling Point: 445.185 °C at 760 mmHg
• Flash Point: 223.04 °C
• PSA: 35.25000
• Density: 1.425g/cm³
• LogP: 5.38920

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Chloro-4-[(3,4-dichlorophenyl)methoxy]benzenamine

There total 2 articles about 3-Chloro-4-[(3,4-dichlorophenyl)methoxy]benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-4-nitrophenol (619-08-9) → C13H10Cl3NO (1039922-08-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 80 °C

2: iron; ammonium chloride / ethanol; water / 2 h / 70 °C

With iron; potassium carbonate; ammonium chloride; In ethanol; water; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2018.06.011

Reference yield:

3,4-Dichlorophenylmethyl chloride (102-47-6) → C13H10Cl3NO (1039922-08-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 80 °C

2: iron; ammonium chloride / ethanol; water / 2 h / 70 °C

With iron; potassium carbonate; ammonium chloride; In ethanol; water; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2018.06.011

Reference yield: 41.0%

4-chloro-6-(4-nitrophenyl)thieno[2,3-d]pyrimidine + C13H10Cl3NO (1039922-08-1) → N-(3-chloro-4-((3,4-dichlorobenzyl)oxy)phenyl)-6-(4-nitrophenyl)thieno[2,3-d]pyrimidin-4-amine

Guidance literature:

In butan-1-ol; at 120 ℃;

DOI:10.1016/j.ejmech.2018.06.011

upstream raw materials:

3,4-Dichlorophenylmethyl chloride

2-chloro-4-nitrophenol

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