4,5-dihydrobenzopyrene-4,5-trans-(e,e)-diol

Base Information

• Chemical Name: 4,5-dihydrobenzo
• Molecular Formula: C₂₀H₁₄O₂
• Molecular Weight: 286.33

Synonyms:

Chemical Property of 4,5-dihydrobenzo

Chemical Property:

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There total 5 articles about 4,5-dihydrobenzopyrene-4,5-trans-(e,e)-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

benzo<α>pyrene-4,5-dione (42286-46-4) → 4,5-dihydrobenzopyrene-4,5-trans-(e,e)-diol (28622-84-6,37571-88-3,50700-50-0,51689-89-5,62600-10-6,64474-18-6,72040-28-9,72040-29-0,72040-30-3)

Guidance literature:

With sodium tetrahydroborate; oxygen; In ethanol; for 24h; Ambient temperature;

DOI:10.1055/s-1982-29834

Reference yield:

4,5-dihydro(epoxy) benzopyrene (37574-47-3,72010-12-9,72010-13-0) → 5-hydroxy-benzo[a]pyrene (24027-84-7) + 4-hydroxybenzoanthracene (37574-48-4) + 4,5-dihydrobenzopyrene-4,5-trans-(e,e)-diol (28622-84-6,37571-88-3,50700-50-0,51689-89-5,62600-10-6,64474-18-6,72040-28-9,72040-29-0,72040-30-3)

Guidance literature:

With ethylenediaminetetraacetic acid; tris hydrochloride; In sodium hydroxide; at 23 ℃; pH=7.3; Kinetics;

DOI:10.1021/tx960134j

Reference yield:

4,5-dihydro(epoxy) benzopyrene (37574-47-3,72010-12-9,72010-13-0) + calf thymus desoxyribonucleic acid → 5-hydroxy-benzo[a]pyrene (24027-84-7) + 4-hydroxybenzoanthracene (37574-48-4) + 4,5-dihydrobenzopyrene-4,5-trans-(e,e)-diol (28622-84-6,37571-88-3,50700-50-0,51689-89-5,62600-10-6,64474-18-6,72040-28-9,72040-29-0,72040-30-3) + 2-(4-Hydroxy-4,5-dihydro-benzo[def]chrysen-5-ylamino)-9-((2R,4S,5R)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1,9-dihydro-purin-6-one

Guidance literature:

With sodium hydroxide; ethylenediaminetetraacetic acid; tris hydrochloride; at 23 ℃; pH=7.3; Kinetics;

DOI:10.1021/tx960134j

upstream raw materials:

4,5-dihydro(epoxy) benzopyrene

benzo<α>pyrene-4,5-dione

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