bis(2,2'-bipyridine)(1-((p-nitrophenyl)azo)-2-naphtholato)ruthenium(II) perchlorate

Base Information

• Chemical Name: bis(2,2'-bipyridine)(1-((p-nitrophenyl)azo)-2-naphtholato)ruthenium(II) perchlorate
• CAS No.: 77590-09-1
• Molecular Formula: C₃₆H₂₆N₇O₃Ru*ClO₄
• Molecular Weight: 805.168
• Mol file: 77590-09-1.mol

Synonyms:

Chemical Property of bis(2,2'-bipyridine)(1-((p-nitrophenyl)azo)-2-naphtholato)ruthenium(II) perchlorate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(2,2'-bipyridine)(1-((p-nitrophenyl)azo)-2-naphtholato)ruthenium(II) perchlorate

There total 1 articles about bis(2,2'-bipyridine)(1-((p-nitrophenyl)azo)-2-naphtholato)ruthenium(II) perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{RuC2O4(bpy)2}*4H2O + sodium perchlorate + para red (6410-10-2) → bis(2,2'-bipyridine)(1-((p-nitrophenyl)azo)-2-naphtholato)ruthenium(II) perchlorate (77590-09-1)

Guidance literature:

With hydrogenchloride; In methanol; To a soln. of complex in MeOH aq. HCl was added, heated to reflux for 12 h, the ligand and NaOH was added, refluxed for 6 h, filtered, NaClO4 in MeOH was added;; reduced in vol., ppt. was filtered, washed with H2O, benzene, ether, dried under vac.; elem. anal.;;

upstream raw materials:

para red

Refernces