1,3-Dimethylcyclohex-2-ene-1,2-dicarbaldehyde

Base Information

Chemical Name:1,3-Dimethylcyclohex-2-ene-1,2-dicarbaldehyde
CAS No.:130735-23-8
Molecular Formula:C₁₀H₁₄O₂
Molecular Weight:166.22
Hs Code.:

Synonyms:

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Chemical Property of 1,3-Dimethylcyclohex-2-ene-1,2-dicarbaldehyde

Chemical Property:

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Technology Process of 1,3-Dimethylcyclohex-2-ene-1,2-dicarbaldehyde

There total 12 articles about 1,3-Dimethylcyclohex-2-ene-1,2-dicarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 130735-22-7
1,3-Dimethylcyclohex-2-ene-1,2-dicarbaldehyde 1-Ethylene Acetal

: 130735-23-8
1,3-Dimethylcyclohex-2-ene-1,2-dicarbaldehyde

Guidance literature:: With acetic acid; at 50 ℃; for 0.5h;
DOI:10.1039/P19900001901

Reference yield:

: 87787-09-5
6-hydroxymethyl-6-methyl-1,4-dioxaspiro<4.5>decane

: 130735-23-8
1,3-Dimethylcyclohex-2-ene-1,2-dicarbaldehyde

Guidance literature:: Multi-step reaction with 10 steps

1: 7.43 g / di-isopropylethylamine / CH₂Cl₂ / Ambient temperature

2: pyridinium toluene-p-sulphonate / acetone / Heating

3: 90 percent / NaH / tetrahydrofuran / 3 h / Heating

4: NaH / 1.) THF, 0 deg C, 30 min, 2. a) 0 deg C, 40 min, b) RT

5: 40 percent / LiCl / hexamethylphosphoric acid triamide / 2 h / 120 °C

6: conc. H₂SO₄ / ethanol / 3 h / Heating

8: 84 percent / D-camphorsulphonic acid / 5 h / 40 °C

10: 50 percent / aq. acetic acid / 0.5 h / 50 °C

With sulfuric acid; camphor-10-sulfonic acid; pyridinium p-toluenesulfonate; sodium hydride; acetic acid; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; acetone;
DOI:10.1039/P19900001901

Reference yield:

: 13839-77-5
Ethyl 6-methyl-1,4-dioxaspiro[4.5]decane-6-carboxylate

: 130735-23-8
1,3-Dimethylcyclohex-2-ene-1,2-dicarbaldehyde

Guidance literature:: Multi-step reaction with 11 steps

1: LiAlH₄ / diethyl ether / 0.5 h / Ambient temperature

2: 7.43 g / di-isopropylethylamine / CH₂Cl₂ / Ambient temperature

3: pyridinium toluene-p-sulphonate / acetone / Heating

4: 90 percent / NaH / tetrahydrofuran / 3 h / Heating

5: NaH / 1.) THF, 0 deg C, 30 min, 2. a) 0 deg C, 40 min, b) RT

6: 40 percent / LiCl / hexamethylphosphoric acid triamide / 2 h / 120 °C

7: conc. H₂SO₄ / ethanol / 3 h / Heating

9: 84 percent / D-camphorsulphonic acid / 5 h / 40 °C

11: 50 percent / aq. acetic acid / 0.5 h / 50 °C

With lithium aluminium tetrahydride; sulfuric acid; camphor-10-sulfonic acid; pyridinium p-toluenesulfonate; sodium hydride; acetic acid; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; ethanol; dichloromethane; acetone;
DOI:10.1039/P19900001901