{CH₂C(CH₂CH₃)COCH₃}Fe(CO)2(P(C₆H₅)3)

Base Information

• Chemical Name: {CH₂C(CH₂CH₃)COCH₃}Fe(CO)2(P(C₆H₅)3)
• CAS No.: 120712-30-3
• Molecular Formula: C₂₆H₂₅FeO₃P
• Molecular Weight: 472.303

Synonyms:

Chemical Property of {CH₂C(CH₂CH₃)COCH₃}Fe(CO)2(P(C₆H₅)3)

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of {CH₂C(CH₂CH₃)COCH₃}Fe(CO)2(P(C₆H₅)3)

There total 2 articles about {CH₂C(CH₂CH₃)COCH₃}Fe(CO)2(P(C₆H₅)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tricarbonyl(η(4)-buta-1,3-diene)iron (522611-42-3,12078-32-9,139687-42-6,71435-61-5) → CHCH3C(CH3)C(O)CH3Fe(CO)2P(C6H5)3 + CHCH3C(CH3)C(O)CH3Fe(CO)2P(C6H5)3 + {CH2C(CH2CH3)COCH3}Fe(CO)2(P(C6H5)3) (120712-30-3)

Guidance literature:

With triphenylphosphine; methyl iodide; In tetrahydrofuran; react. of the starting compds. at 0°C, addn. of CH3I, stirring for 5 min, addn. of the phosphine, stirring for 2 h at 25°C; quenching with water, extn. with ether, dried over MgSO4, filtn. through silica gel, evapn. of the solvent, purifn. by column chromy. on silica gel with petrol ether/ether;

Reference yield:

η3-syn-methallyl iron tricarbonyl iodide → CHCH3C(CH3)C(O)CH3Fe(CO)2P(C6H5)3 + CHCH3C(CH3)C(O)CH3Fe(CO)2P(C6H5)3 + {CH2C(CH2CH3)COCH3}Fe(CO)2(P(C6H5)3) (120712-30-3)

Guidance literature:

With sodium amalgam; triphenylphosphine; methyl iodide; In tetrahydrofuran; soln. of syn-methallyl iron tricarbonyl iodide is dropwise added to stirring Na-amalgam at 0°C, addn. of CH3I at 0°C, stirring for 20 min at 0°C, addn. of the phosphine, stirring for 2 h at 25°C; purifn. by column chromy. using CH2Cl2/hexane;

upstream raw materials:

tricarbonyl(η(4)-buta-1,3-diene)iron

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