Technology Process of 1,2:3,4-di-μ(2)-2-[(3-chloro-2-methylphenyl)amino]benzoato-O,O-1,3-bis-2-[(3-chloro-2-methylphenyl)amino]benzoato-O-1,2,4:2,3,4-di-μ(3)-oxo-tetrakis[di-n-butyltin(IV)]
There total 1 articles about 1,2:3,4-di-μ(2)-2-[(3-chloro-2-methylphenyl)amino]benzoato-O,O-1,3-bis-2-[(3-chloro-2-methylphenyl)amino]benzoato-O-1,2,4:2,3,4-di-μ(3)-oxo-tetrakis[di-n-butyltin(IV)] which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
benzene;
organotin oxide (1.2 mmol) and tolfenamic acid (1 mmol) refluxed in benzene overnight with azeotropic removal of water; soln. concd. to a small vol.; drops of Et2O added; slow evapn.; crystalssepd. off; elem. anal.;
DOI:10.1016/S0022-328X(00)00819-6