pentakis(benzyl isocyanide)(2,2'-bipyridine)molybdenum(II) dihexafluorophosphate

Base Information

Chemical Name:pentakis(benzyl isocyanide)(2,2'-bipyridine)molybdenum(II) dihexafluorophosphate
CAS No.:90885-45-3
Molecular Formula:C₅₀H₄₃MoN₇*2F₆P
Molecular Weight:1127.81
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentakis(benzyl isocyanide)(2,2'-bipyridine)molybdenum(II) dihexafluorophosphate

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Technology Process of pentakis(benzyl isocyanide)(2,2'-bipyridine)molybdenum(II) dihexafluorophosphate

There total 1 articles about pentakis(benzyl isocyanide)(2,2'-bipyridine)molybdenum(II) dihexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 15668-64-1
tetracarbonyl(2,2'-bipyridine)molybdenum

: 88333-03-3,10340-91-7
Benzyl isocyanide

: 90885-45-3
pentakis(benzyl isocyanide)(2,2'-bipyridine)molybdenum(II) dihexafluorophosphate

Guidance literature:: With potassium hexafluorophosphate; (Dichloroiodo)benzene; In methanol; byproducts: CO; (N2); satd. Mo complex soln. stirred for 15 min at room temp. in darkness, solid C6H5ICl2 added, stirred for 30 min at room temp., ligand syringed, stirred at room temp. for 16 h; filtered into KPF6/acetone soln., pptd. under stream of N2, filtered, washed with H2O, Et2O and MeOH, recrystd. (MeOH/Et2O); elem. anal.;
DOI:10.1016/0022-328X(84)85038-X

Reference yield:

: 90885-45-3
pentakis(benzyl isocyanide)(2,2'-bipyridine)molybdenum(II) dihexafluorophosphate

: [(Mo(benzyl isocyanide)4(2,2'-bipyridine))2(μ-CN)](PF6)3

Guidance literature:: With potassium hexafluorophosphate; In not given; (N2); Mo complex and KPF6 refluxed in solvent for up to 3 d;
DOI:10.1016/0022-328X(84)85038-X