5-FORMYL-2-ISOPROXYPYRIDINE

Base Information

• Chemical Name: 5-FORMYL-2-ISOPROXYPYRIDINE
• CAS No.: 884495-35-6
• Molecular Formula: C₉H₁₁NO₂
• Molecular Weight: 165.192
• Hs Code.: 2933399090
• Mol file: 884495-35-6.mol

Synonyms:6-Isopropoxynicotinaldehyde;

Chemical Property of 5-FORMYL-2-ISOPROXYPYRIDINE

Chemical Property:

• Boiling Point: 266℃
• Flash Point: 115℃
• PSA: 39.19000
• Density: 1.088
• LogP: 1.68130
• Storage Temp.: Inert atmosphere,Store in freezer, under -20°C

Purity/Quality:

99% ^*data from raw suppliers

5-Formyl-2-isoproxypyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-FORMYL-2-ISOPROXYPYRIDINE

There total 1 articles about 5-FORMYL-2-ISOPROXYPYRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-bromo-2-isopropoxy-pyridine (870521-31-6) + N-methoxy-N-methyl-formamide (32117-82-1) → 6-(1-methylethoxy)-3-pyridinecarbaldehyde (884495-35-6)

Guidance literature:

5-bromo-2-isopropoxy-pyridine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

N-methoxy-N-methyl-formamide; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

Reference yield:

6-(1-methylethoxy)-3-pyridinecarbaldehyde (884495-35-6) → 2-isopropoxy-5-(4-((3-(trifluoromethyl)phenyl)thio)tetrahydro-2H-pyran-2-yl)pyridine

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane / 3 h / 0 °C

2: potassium carbonate / acetonitrile / 67 h / 50 °C / Inert atmosphere

With potassium carbonate; In dichloromethane; acetonitrile;

Reference yield:

6-(1-methylethoxy)-3-pyridinecarbaldehyde (884495-35-6) → 2-isopropoxy-5-(4-((3-(trifluoromethyl)phenyl)sulfonyl)tetrahydro-2H-pyran-2-yl)pyridine

Guidance literature:

Multi-step reaction with 3 steps

1: dichloromethane / 3 h / 0 °C

2: potassium carbonate / acetonitrile / 67 h / 50 °C / Inert atmosphere

3: Oxone / methanol; water / 19 h / 0 - 23 °C

With Oxone; potassium carbonate; In methanol; dichloromethane; water; acetonitrile;

upstream raw materials:

5-bromo-2-isopropoxy-pyridine

N-methoxy-N-methyl-formamide

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