ethyl 2-benzyloxycarbonylamino-2-malonate

Base Information

Chemical Name:ethyl 2-benzyloxycarbonylamino-2-malonate
CAS No.:129243-64-7
Molecular Formula:C₂₃H₂₈N₂O₈
Molecular Weight:460.484
Hs Code.:

ethyl 2-benzyloxycarbonylamino-2-<N-(t-butoxycarbonyl)-pyrrol-2-ylmethyl>malonate

Synonyms:

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Chemical Property of ethyl 2-benzyloxycarbonylamino-2-malonate

Chemical Property:

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Technology Process of ethyl 2-benzyloxycarbonylamino-2-malonate

There total 6 articles about ethyl 2-benzyloxycarbonylamino-2-malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3072-56-8
2-(diethylaminomethyl)pyrrole

: 129243-64-7
ethyl 2-benzyloxycarbonylamino-2-malonate

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / ethanol / 2 h

2: 1) Na, EtOH / 2) reflux, 2h

3: 97 percent / dimethylaminopyridine / acetonitrile / 16 h / Ambient temperature

4: 74 percent / 1M NaOH / ethanol / 2 h

With dmap; sodium hydroxide; ethanol; sodium; In ethanol; acetonitrile;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 129243-64-7
ethyl 2-benzyloxycarbonylamino-2-malonate

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / dimethylaminopyridine / acetonitrile / 16 h / Ambient temperature

2: 74 percent / 1M NaOH / ethanol / 2 h

With dmap; sodium hydroxide; In ethanol; acetonitrile;

Reference yield:

: 3005-66-1
diethyl 2-benzyloxycarbonylaminomalonate

: 129243-64-7
ethyl 2-benzyloxycarbonylamino-2-malonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Na, EtOH / 2) reflux, 2h

2: 97 percent / dimethylaminopyridine / acetonitrile / 16 h / Ambient temperature

3: 74 percent / 1M NaOH / ethanol / 2 h

With dmap; sodium hydroxide; ethanol; sodium; In ethanol; acetonitrile;