4-chlorobenzylamine trifluoroacetate

Base Information

Chemical Name:4-chlorobenzylamine trifluoroacetate
CAS No.:125687-16-3
Molecular Formula:C₂HF₃O₂*C₇H₈ClN
Molecular Weight:255.624
Hs Code.:

Synonyms:

Suppliers and Price of 4-chlorobenzylamine trifluoroacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chlorobenzylamine trifluoroacetate

Chemical Property:

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Technology Process of 4-chlorobenzylamine trifluoroacetate

There total 2 articles about 4-chlorobenzylamine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1117-74-4
4-oxohexanoic acid

: 103252-87-5
1-[(4-chlorophenyl)methyl]-1-(phenyl)hydrazine hydrochloride

: 125687-13-0
3-(3-methyl-1H-indol-2-yl)propanoic acid

: 103252-86-4
3-[1-(4-chlorobenzyl)-3-methylindol-2-yl]propionic acid

: 125687-16-3
4-chlorobenzylamine trifluoroacetate

Guidance literature:: With trifluoroacetic acid; In tert-butyl alcohol; at 80 ℃; for 23.75h; free hydrazine from hydrochloride and 1 N NaOH in toluene;
DOI:10.1021/jo00296a063

Reference yield:

: 104-83-6
1-Chloro-4-(chloromethyl)benzene

: 125687-16-3
4-chlorobenzylamine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / 1.) triethylamine, 2.) HCl gas / toluene / 6 h / Heating

2: CF₃COOH / 2-methyl-propan-2-ol / 23.75 h / 80 °C / free hydrazine from hydrochloride and 1 N NaOH in toluene

With hydrogenchloride; triethylamine; trifluoroacetic acid; In toluene; tert-butyl alcohol;
DOI:10.1021/jo00296a063