3-(Methoxymethyl)azetidine hydrochloride

Base Information

• Chemical Name: 3-(Methoxymethyl)azetidine hydrochloride
• CAS No.: 942308-06-7
• Molecular Formula: C5H12ClNO
• Molecular Weight: 137.609
• Hs Code.: 2933990090
• Mol file: 942308-06-7.mol

Synonyms:3-(METHOXYMETHYL)AZETIDINE HYDROCHLORIDE;3-(methoxymethyl)azetidine;3-(Methoxymethyl)-azetidi...;3-(MethoxyMethyl)azetidine-HCl;3-(Methoxymethyl)azetane hydrochloride

Chemical Property of 3-(Methoxymethyl)azetidine hydrochloride

Chemical Property:

• PSA: 21.26000
• LogP: 0.98300
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

3-(Methoxymethyl)azetidinehydrochloride 97.0% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(Methoxymethyl)azetidine hydrochloride

There total 1 articles about 3-(Methoxymethyl)azetidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methoxymethyl-azetidine-1-carboxylic acid tert-butyl ester (942308-05-6) → 3-(methoxymethyl)azetidine hydrochloride (942308-06-7)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 72h;

Reference yield: 22.0%

3-(methoxymethyl)azetidine hydrochloride (942308-06-7) + 3-methyl-2-[(1R)-1-(4-oxocyclohexyl)ethyl]-6,7-dihydrothieno[3,2-c]pyridin-4(5H)-one → 2-[(1R)-1-{trans-4-[3-(methoxymethyl)azetidin-1-yl]cyclohexyl}ethyl]-3-methyl-6,7-dihydrothieno[3,2-c]pyridin-4(5H)-one

Guidance literature:

3-(methoxymethyl)azetidine hydrochloride; With N-ethyl-N,N-diisopropylamine; In methanol; at 20 ℃; for 0.166667h; Inert atmosphere;

3-methyl-2-[(1R)-1-(4-oxocyclohexyl)ethyl]-6,7-dihydrothieno[3,2-c]pyridin-4(5H)-one; In methanol; for 4h;

With lithium borohydride; In tetrahydrofuran; methanol; at -78 - 20 ℃;

Reference yield: 21.0%

3-(methoxymethyl)azetidine hydrochloride (942308-06-7) + (S)-3,4-difluoro-N-methyl-N-(3-methyl-1-oxobutan-2-yl)benzamide (1380104-50-6) → (S)-3,4-difluoro-N-(1-(3-(methoxymethyl)azetidin-1-yl)-3-methylbutan-2-yl)-N-methylbenzamide (1380102-21-5)

Guidance literature:

With sodium cyanoborohydride; triethylamine; In methanol; at 20 ℃;

upstream raw materials:

3-methoxymethyl-azetidine-1-carboxylic acid tert-butyl ester

Downstream raw materials:

(S)-3,4-difluoro-N-(1-(3-(methoxymethyl)azetidin-1-yl)-3-methylbutan-2-yl)-N-methylbenzamide

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