pentaphenylcyclopentadienylthallium

Base Information

• Chemical Name: pentaphenylcyclopentadienylthallium
• CAS No.: 115261-86-4
• Molecular Formula: C₃₅H₂₅Tl
• Molecular Weight: 649.966
• Mol file: 115261-86-4.mol

Synonyms:

Chemical Property of pentaphenylcyclopentadienylthallium

Chemical Property:

Purity/Quality:

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Technology Process of pentaphenylcyclopentadienylthallium

There total 1 articles about pentaphenylcyclopentadienylthallium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1,2,3,4,5-pentaphenylcyclopentadiene (2519-10-0) + thallium (I) ethoxide (20398-06-5) → pentaphenylcyclopentadienylthallium (115261-86-4)

Guidance literature:

In toluene; byproducts: C2H5OH; under N2, cyclopentadiene suspended in toluene at 110°C, dropwise addn. of TlOC2H5 and toluene during 1 h with rapid stirring, stirred for 30 min; pptn. filtered off, dried in vac. (over night, room temp.); elem. anal.;

DOI:10.1016/S0022-328X(00)99048-X

upstream raw materials:

1,2,3,4,5-pentaphenylcyclopentadiene

thallium (I) ethoxide

Refernces