4-bromo-1H-pyrrolo[2,3-c]pyridine

Base Information

Chemical Name:4-bromo-1H-pyrrolo[2,3-c]pyridine
CAS No.:69872-17-9
Molecular Formula:C7H5BrN2
Molecular Weight:197.034
Hs Code.:2933990090
European Community (EC) Number:867-030-1
DSSTox Substance ID:DTXSID60500854
Wikidata:Q72512308
Mol file:69872-17-9.mol

Synonyms:4-bromo-1H-pyrrolo[2,3-c]pyridine;69872-17-9;4-Bromo-6-azaindole;MFCD11847768;1H-Pyrrolo[2,3-c]pyridine, 4-bromo-;SCHEMBL529739;DTXSID60500854;NZUWATDXQMWXMY-UHFFFAOYSA-N;AKOS007930881;CS-W019705;FS-3369;PB31599;AC-22993;SY028295;4-bromo-1H-pyrrolo[2 pound not3-c]pyridine;A9239;AM20061454;FT-0658920;EN300-155130;J-514557;Z1255357182

Suppliers and Price of 4-bromo-1H-pyrrolo[2,3-c]pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Bromo-1H-pyrrolo[2,3-c]pyridine
250mg
$ 75.00

SynQuest Laboratories
4-Bromo-1H-pyrrolo[2,3-c]pyridine 97%
1 g
$ 69.00

Matrix Scientific
4-Bromo-1H-pyrrolo[2,3-c]pyridine 95%
5g
$ 485.00

Matrix Scientific
4-Bromo-1H-pyrrolo[2,3-c]pyridine 95%
1g
$ 147.00

J&W Pharmlab
4-Bromo-1H-pyrrolo[2,3-c]pyridine 96%
1g
$ 75.00

J&W Pharmlab
4-Bromo-1H-pyrrolo[2,3-c]pyridine 96%
5g
$ 255.00

J&W Pharmlab
4-Bromo-1H-pyrrolo[2,3-c]pyridine 96%
25g
$ 895.00

Crysdot
4-Bromo-1H-pyrrolo[2,3-c]pyridine 98%
10g
$ 300.00

Crysdot
4-Bromo-1H-pyrrolo[2,3-c]pyridine 98%
25g
$ 600.00

Crysdot
4-Bromo-1H-pyrrolo[2,3-c]pyridine 98%
5g
$ 165.00

Total 71 raw suppliers

Chemical Property of 4-bromo-1H-pyrrolo[2,3-c]pyridine

Chemical Property:

Appearance/Colour:light yellow solid
Vapor Pressure:0mmHg at 25°C
Melting Point:188-189℃
Refractive Index:1.728
Boiling Point:337.619 °C at 760 mmHg
PKA:13.73±0.40(Predicted)
Flash Point:157.986 °C
PSA：28.68000
Density:1.771 g/cm³
LogP:2.32540
Storage Temp.:2-8°C(protect from light)
XLogP3:1.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:195.96361
Heavy Atom Count:10
Complexity:129

Purity/Quality:

99%, ^*data from raw suppliers

4-Bromo-1H-pyrrolo[2,3-c]pyridine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CNC2=CN=CC(=C21)Br

Technology Process of 4-bromo-1H-pyrrolo[2,3-c]pyridine

There total 9 articles about 4-bromo-1H-pyrrolo[2,3-c]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 69872-16-8
[2-(3-bromo-5-nitro-pyridin-4-yl)-vinyl]-dimethyl-amine

: 69872-17-9
4-bromo-1H-pyrrolo[2,3-c]pyridine

Guidance literature:: With iron; acetic acid; at 120 ℃;
DOI:10.1002/hlca.202100211

Reference yield: 73.0%

: 1258875-12-5
(E)-2-(3-bromo-5-nitro-4-pyridinyl)-N,N-dimethylethenamine

: 69872-17-9
4-bromo-1H-pyrrolo[2,3-c]pyridine

Guidance literature:: With iron; acetic acid; for 0.75h; Heating / reflux;

Reference yield:

: 5435-54-1
4-hydroxy-3-nitropyridine

: 69872-17-9
4-bromo-1H-pyrrolo[2,3-c]pyridine

Guidance literature:: Multi-step reaction with 6 steps

1.1: bromine / water / 2 h / 50 °C

2.1: diethylamine; trichlorophosphate / 5 h / Reflux

3.1: sodium hydride / N,N-dimethyl-formamide / 0 °C

3.2: 1 h / 0 °C

4.1: hydrogenchloride; water / 16 h / Reflux

5.1: N,N-dimethyl-formamide / 4 h / 90 °C

6.1: iron; acetic acid / 3 h / 90 °C

With hydrogenchloride; water; bromine; iron; sodium hydride; acetic acid; diethylamine; trichlorophosphate; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.11.070