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(C4H2N)3(C4H2N(CC(C6(2)H4Cl)2))(C(C6H5))4FeI

Base Information
  • Chemical Name:(C4H2N)3(C4H2N(CC(C6(2)H4Cl)2))(C(C6H5))4FeI
  • CAS No.:97170-30-4
  • Molecular Formula:C58H36Cl2FeIN4
  • Molecular Weight:1050.54
  • Hs Code.:
(C<sub>4</sub>H<sub>2</sub>N)3(C<sub>4</sub>H<sub>2</sub>N(CC(C<sub>6</sub><sup>(2)</sup>H<sub>4</sub>Cl)2))(C(C<sub>6</sub>H<sub>5</sub>))4FeI

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Chemical Property of (C4H2N)3(C4H2N(CC(C6(2)H4Cl)2))(C(C6H5))4FeI
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Technology Process of (C4H2N)3(C4H2N(CC(C6(2)H4Cl)2))(C(C6H5))4FeI

There total 2 articles about (C4H2N)3(C4H2N(CC(C6(2)H4Cl)2))(C(C6H5))4FeI which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With iodine; In benzene; addn. of I2 in benzene to the starting complex in benzene within 1 h;;
Guidance literature:
With air; iron; In methanol; dichloromethane; stirring of the starting Fe(III)-complex with Fe-powder in CH2Cl2-methanol for 30 min under Ar, addn. of the trichloroethane over 2 h, stirring for 30 min, filtn., filtrate is washed with water containing sodium dithionite, oxidn. with air;; removal of the solvent by evapn., chromy., recrystn. of the residue (acetone/hexane);;
Guidance literature:
With sodium azide; In water; benzene; stirring of an aq. soln. of the sodium salt in water with a benzene soln. of the starting complex for 2 h;; benzene soln. is separated, evapn. to dryness, redissolving of the residue in acetone, filtn., pptn. with hexane;;
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