cis-1,1,2-trimethyl-5-phenylpyrrolidinium bromide

Base Information

Chemical Name:cis-1,1,2-trimethyl-5-phenylpyrrolidinium bromide
CAS No.:104920-99-2
Molecular Formula:Br*C₁₃H₂₀N
Molecular Weight:270.213
Hs Code.:

Synonyms:

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Chemical Property of cis-1,1,2-trimethyl-5-phenylpyrrolidinium bromide

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Technology Process of cis-1,1,2-trimethyl-5-phenylpyrrolidinium bromide

There total 8 articles about cis-1,1,2-trimethyl-5-phenylpyrrolidinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3240-29-7
1-Phenylpent-4-en-1-one

: 104920-99-2,113579-91-2,113579-92-3
cis-1,1,2-trimethyl-5-phenylpyrrolidinium bromide

Guidance literature:: Multi-step reaction with 5 steps

1: magnesium sulfate / diethyl ether / 70 - 80 °C / autoclave

2: sodium borohydride (NaBH₄) / methanol / Ambient temperature

3: butyllithium / tetrahydrofuran / 0.5 h / -10 °C

4: 0.25M lithium perchlorate / tetrahydrofuran; hexamethylphosphoric acid triamide / -10 °C / anodic oxidation

5: diethyl ether / 3 h

With sodium tetrahydroborate; n-butyllithium; lithium perchlorate; magnesium sulfate; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether;
DOI:10.1016/S0040-4020(01)89956-7

Reference yield:

: 102632-99-5,134679-60-0,144178-31-4,54525-86-9
1-phenyl-4-penten-1-ol

: 104920-99-2,113579-91-2,113579-92-3
cis-1,1,2-trimethyl-5-phenylpyrrolidinium bromide

Guidance literature:: Multi-step reaction with 6 steps

1: pyridinium chlorochromate (PCC) / CH₂Cl₂ / 3 h / Heating

2: magnesium sulfate / diethyl ether / 70 - 80 °C / autoclave

3: sodium borohydride (NaBH₄) / methanol / Ambient temperature

4: butyllithium / tetrahydrofuran / 0.5 h / -10 °C

5: 0.25M lithium perchlorate / tetrahydrofuran; hexamethylphosphoric acid triamide / -10 °C / anodic oxidation

6: diethyl ether / 3 h

With sodium tetrahydroborate; n-butyllithium; lithium perchlorate; magnesium sulfate; pyridinium chlorochromate; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)89956-7

Reference yield:

: 104886-43-3
N-methyl-1-phenylpent-4-en-1-amine

: 104920-99-2,113579-91-2,113579-92-3
cis-1,1,2-trimethyl-5-phenylpyrrolidinium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: butyllithium / tetrahydrofuran / 0.5 h / -10 °C

2: 0.25M lithium perchlorate / tetrahydrofuran; hexamethylphosphoric acid triamide / -10 °C / anodic oxidation

3: diethyl ether / 3 h

With n-butyllithium; lithium perchlorate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether;
DOI:10.1016/S0040-4020(01)89956-7