C₃₀H₃₃NO₉

Base Information

Chemical Name:C₃₀H₃₃NO₉
CAS No.:1280608-59-4
Molecular Formula:C₃₀H₃₃NO₉
Molecular Weight:551.593
Hs Code.:

C<sub>30</sub>H<sub>33</sub>NO<sub>9</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₃₃NO₉

Chemical Property:

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Technology Process of C₃₀H₃₃NO₉

There total 6 articles about C₃₀H₃₃NO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1280608-57-2
C₃₀H₃₅NO₉

: 1280608-59-4
C₃₀H₃₃NO₉

: C₃₀H₃₃NO₉

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 0 - 20 ℃; Molecular sieve;
DOI:10.1002/anie.201006528

Reference yield:

: 1280608-40-3
C₂₃H₂₅NO₆

: 1280608-59-4
C₃₀H₃₃NO₉

: C₃₀H₃₃NO₉

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

2.2: 2.5 h / 20 °C

3.1: Oxone; C₁₃H₂₀O₉; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer

4.1: water; pyridinium p-toluenesulfonate / 1,4-dioxane / 12 h / 70 °C

5.1: [bis(acetoxy)iodo]benzene; potassium hydroxide / 2 h / 0 °C

6.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

With Oxone; sodium tetrahydroborate; tetrapropylammonium perruthennate; C₁₃H₂₀O₉; [bis(acetoxy)iodo]benzene; water; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; sodium hydride; potassium carbonate; 4-methylmorpholine N-oxide; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; Dimethoxymethane; dichloromethane; water; acetonitrile; mineral oil; 3.1: Shi epoxidation;
DOI:10.1002/anie.201006528

Reference yield:

: 1280608-50-5
C₂₃H₂₇NO₆

: 1280608-59-4
C₃₀H₃₃NO₉

: C₃₀H₃₃NO₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

1.2: 2.5 h / 20 °C

2.1: Oxone; C₁₃H₂₀O₉; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer

3.1: water; pyridinium p-toluenesulfonate / 1,4-dioxane / 12 h / 70 °C

4.1: [bis(acetoxy)iodo]benzene; potassium hydroxide / 2 h / 0 °C

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

With Oxone; tetrapropylammonium perruthennate; C₁₃H₂₀O₉; [bis(acetoxy)iodo]benzene; water; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; sodium hydride; potassium carbonate; 4-methylmorpholine N-oxide; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; Dimethoxymethane; dichloromethane; water; acetonitrile; mineral oil; 2.1: Shi epoxidation;
DOI:10.1002/anie.201006528