Technology Process of C22H25N5OS
There total 5 articles about C22H25N5OS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
2: hydrogenchloride / water; acetone / 1 h / 60 °C
3: morpholine; octasulfur / tetrahydrofuran; ethanol / 1 h / 20 °C
4: sulfuric acid / 3 h / 40 °C
With
morpholine; hydrogenchloride; octasulfur; sulfuric acid; trifluoroacetic acid;
In
tetrahydrofuran; ethanol; dichloromethane; water; acetone;
3: Gewald reaction;
DOI:10.1016/j.bmcl.2011.01.069
- Guidance literature:
-
Multi-step reaction with 2 steps
1: morpholine; octasulfur / tetrahydrofuran; ethanol / 1 h / 20 °C
2: sulfuric acid / 3 h / 40 °C
With
morpholine; octasulfur; sulfuric acid;
In
tetrahydrofuran; ethanol;
1: Gewald reaction;
DOI:10.1016/j.bmcl.2011.01.069
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride / water; acetone / 1 h / 60 °C
2: morpholine; octasulfur / tetrahydrofuran; ethanol / 1 h / 20 °C
3: sulfuric acid / 3 h / 40 °C
With
morpholine; hydrogenchloride; octasulfur; sulfuric acid;
In
tetrahydrofuran; ethanol; water; acetone;
2: Gewald reaction;
DOI:10.1016/j.bmcl.2011.01.069