sambutoxin

Base Information

• Chemical Name: sambutoxin
• CAS No.: 160047-56-3
• Molecular Formula: C₂₈H₃₉NO₄
• Molecular Weight: 453.622
• Mol file: 160047-56-3.mol

Synonyms:2(1H)-Pyridinone,4-hydroxy-5-(4-hydroxyphenyl)-1-methyl-3-[(2S,5R,6R)-tetrahydro-5-methyl-6-[(1E,3R,5S)-1,3,5-trimethyl-1-heptenyl]-2H-pyran-2-yl]-(9CI); (-)-Sambutoxin; Sambutoxin

Chemical Property of sambutoxin

Chemical Property:

• Vapor Pressure: 7.35E-15mmHg at 25°C
• Boiling Point: 592°C at 760 mmHg
• Flash Point: 311.8°C
• PSA: 71.69000
• Density: 1.118g/cm³
• LogP: 6.33830

Purity/Quality:

98%min ^*data from raw suppliers

Sambutoxin 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of sambutoxin

There total 24 articles about sambutoxin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

(-)-oxysporidinone (184871-55-4) → (-)-sambutoxin (160047-56-3) + (-)-1'(6')-dehydro-4,6'-anhydrooxysporidinone

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 0.5h;

DOI:10.1016/j.bmcl.2011.02.091

Reference yield: 38.0%

(-)-fusoxypyridone → (-)-sambutoxin (160047-56-3) + (-)-1'(6')-dehydro-4,6'-anhydrooxysporidinone

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 25 ℃; for 0.5h;

DOI:10.1016/j.bmcl.2011.02.091

Reference yield:

4-Hydroxy-5-(4-methoxymethoxy-phenyl)-1-methyl-3-[(2R,5S,6S)-5-methyl-6-((E)-(3S,5R)-1,3,5-trimethyl-hept-1-enyl)-tetrahydro-pyran-2-yl]-1H-pyridin-2-one (306275-14-9) → (+)-sambutoxin (160047-56-3)

Guidance literature:

With hydrogenchloride; sodium iodide; In water; acetone; at 22 ℃;

DOI:10.1021/ol006410+

upstream raw materials:

4-Hydroxy-5-(4-methoxymethoxy-phenyl)-1-methyl-3-[(2R,5S,6S)-5-methyl-6-((E)-(3S,5R)-1,3,5-trimethyl-hept-1-enyl)-tetrahydro-pyran-2-yl]-1H-pyridin-2-one

(2E,4S,6R)-2,4,6-trimethyl-2-octenal

(E)-(4S,6R)-2,4,6-Trimethyl-oct-2-en-1-ol

(E)-(2S,3S,6S,8R)-3-(tert-Butyl-dimethyl-silanyloxy)-2,4,6,8-tetramethyl-dec-4-en-1-ol

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