bis(tetraphenylantimony) sulfate

Base Information

• Chemical Name: bis(tetraphenylantimony) sulfate
• CAS No.: 728916-09-4
• Molecular Formula: C₄₈H₄₀O₄SSb₂
• Molecular Weight: 956.409
• Mol file: 728916-09-4.mol

Synonyms:

Chemical Property of bis(tetraphenylantimony) sulfate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(tetraphenylantimony) sulfate

There total 3 articles about bis(tetraphenylantimony) sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

triphenylantimony sulfate (98529-41-0) + pentaphenylantimony (2170-05-0) → bis(tetraphenylantimony) sulfate (728916-09-4,3223-05-0,26070-06-4)

Guidance literature:

In toluene; mixt. of SbPh5 and of SbPh3SO4 in toluene heated at 90-100°C for 6 h in glass evacuated ampoule; solvent removed; residue dissolved in hot water and soln. filtered off; solvent evapd. and (Ph4Sb)2SO4 was obtained;

DOI:10.1023/A:1022377815791

Reference yield: 79.0%

tetraphenylantimony bisulfate + pentaphenylantimony (2170-05-0) → bis(tetraphenylantimony) sulfate (728916-09-4,3223-05-0,26070-06-4)

Guidance literature:

In toluene; react. mixt. kept at 90°C for 1 h; evapd., elem. anal.;

DOI:10.1023/B:RUCO.0000011636.28262.d3

Reference yield: 53.0%

triphenylantimony sulfate + pentaphenylantimony (2170-05-0) → bis(tetraphenylantimony) sulfate (728916-09-4,3223-05-0,26070-06-4)

Guidance literature:

In toluene; react. mixt. kept at 90°C for 4 h; evapd., recrystd. (water), elem. anal.;

DOI:10.1023/B:RUCO.0000011636.28262.d3

upstream raw materials:

pentaphenylantimony

triphenylantimony sulfate